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Microstructural Evolution of Oxidation Film on a Single Crystal Nickel-Based Superalloy at 980 °C

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Abstract

The isothermal oxidation behavior of a single crystal nickel-based superalloy was investigated at 980 °C through XRD, SEM/EDX and EPMA. The mass gain process exhibited two periods: an initial stage followed by a steady-state stage. Based on the experimental results, the rapid formation of alumina and NiO was responsible for the initial stage of mass gain, and the formation of complex spinels phases may dramatically effect on the steady stage. The microstructure of oxidation film, from the top surface down to the base material, was clarified as Ni-rich oxides, Ni–Cr oxides, Cr–Ta–Co oxides, Ni–Al oxides and finally a continuous Al2O3. In addition, AlN formed in the γ′-free zone. The effect of oxidation film evolution on the oxidation kinetics and mechanism were discussed.

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Acknowledgements

This work has been supported by the NNSF of China (Grant number: U1610256) and 863 program (2105AA034402). These supports are gratefully acknowledged.

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Authors and Affiliations

  1. School of Materials Science and Engineering, Dalian University of Technology, No. 2 Linggong Road, Ganjingzi District, Dalian, 116024, People’s Republic of China

    Yebing Hu, Congqian Cheng, Tieshan Cao & Jie Zhao

  2. Beijing Institute of Aeronautical Materials, Beijing, 100095, People’s Republic of China

    Li Zhang & Guangping Guo

  3. China Automotive Technology Research Center, Tianjin, 300300, People’s Republic of China

    Xianming Meng

Authors
  1. Yebing Hu
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  2. Congqian Cheng
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  3. Li Zhang
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  4. Tieshan Cao
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  5. Guangping Guo
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  6. Xianming Meng
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  7. Jie Zhao
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Correspondence to Jie Zhao.

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Hu, Y., Cheng, C., Zhang, L. et al. Microstructural Evolution of Oxidation Film on a Single Crystal Nickel-Based Superalloy at 980 °C. Oxid Met 89, 303–317 (2018). https://doi.org/10.1007/s11085-017-9787-4

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  • DOI: https://doi.org/10.1007/s11085-017-9787-4

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