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Three-Dimensional Damage Evolution Measurement in EB-PVD TBCs Using Synchrotron Laminography

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Abstract

This study provides the first results of three dimensional microstructural evolution analysis of a typical EB-PVD thermal barrier coating subjected to thermal cycling. Results have been obtained using the technique of synchrotron-radiation computed laminography (SRCL), enabling the scanning of samples that are thin but extended in two dimensions. A correlation with quantitative measurements of phase transformation from β-NiAl to γ’-Ni3Al was achieved from 3D images and 2D cross-section analysis. Morphological features of phase transformation and damaged areas within the bond-coat layer obtained by SRCL are discussed.

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Acknowledgments

Steve Duvinage and Matthieu Rambaudon (Centre des Matériaux) are gratefully acknowledged for specimen preparation and thermal cycling experiment. Pierre Sallot (Centre des Matériaux/Safran) is also acknowledged for precious advice given for specimen preparation for optical observations.

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Authors and Affiliations

  1. Centre des Matériaux, Mines ParisTech, UMR CNRS 7633, BP 87, 91003, Evry Cedex, France

    Vincent Maurel, Romain Soulignac, Thilo F. Morgeneyer, Alain Koster & Luc Rémy

  2. Institute for Photon Science and Synchrotron Radiation (ISS/ANKA), Karlsruhe Institute of Technology, PO Box 3640, 76021, Karlsruhe, Germany

    Lukas Helfen

  3. European Synchrotron Radiation Facility (ESRF), 6 rue Jules Horowitz, BP 220, 38043, Grenoble, France

    Lukas Helfen

  4. SNECMA/SAFRAN Group YQMM, Rond point René Ravaud, 77500, Moissy-Cramayel, France

    Romain Soulignac

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  1. Vincent Maurel
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  2. Lukas Helfen
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  3. Romain Soulignac
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  4. Thilo F. Morgeneyer
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  5. Alain Koster
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  6. Luc Rémy
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Correspondence to Vincent Maurel.

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Maurel, V., Helfen, L., Soulignac, R. et al. Three-Dimensional Damage Evolution Measurement in EB-PVD TBCs Using Synchrotron Laminography. Oxid Met 79, 313–323 (2013). https://doi.org/10.1007/s11085-012-9333-3

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  • DOI: https://doi.org/10.1007/s11085-012-9333-3

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