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GET 133-2023 State Primary Special Standard for the unit of heat in the field of solution and reaction calorimetry

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Measurement Techniques Aims and scope

Abstract

The article shows the need to develop methods and means of reproducing and transferring the unit of heat in the field of measuring the low heat of physicochemical interactions via isothermal titration calorimetry. The relevance of this work is attributable to the wide application of isothermal titration calorimeters implementing this method and the lack of standard metrological procedures and tools designed for metrological support. In order to ensure the uniformity and traceability of measurement in this field, the Calorimetry Laboratory of VNIIM conducted studies to expand the functional and measurement capabilities of GET 133-2012 State Primary Special Standard for the unit of heat in the field of solution and reaction calorimetry. In the course of work, a standard titration microcalorimeter was developed, studied, and included in the improved GET 133-2012; the titration microcalorimeter is designed to reproduce, maintain, and transfer the unit of heat in the field of measuring low heat in liquid media. The studies of the titration microcalorimeter confirmed the possibility of reproducing and transferring the unit of heat within the range of 100–5000 µJ with an expanded uncertainty of 1.2–8.6%. The improved GET 133-2012 having revised composition and new metrological characteristics was approved as GET 133-2023 State Primary Special Standard for the unit of heat in the field of solution and reaction calorimetry. The expansion of the standards base for isothermal titration calorimetry provided the basis for creating new metrological means of transferring the unit of heat in the field of solution and reaction calorimetry.

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Authors and Affiliations

  1. D.I. Mendeleev Institute for Metrology, St. Petersburg, Russian Federation

    K. A. Mishina, E. N. Korchagina & I. V. Kazartsev

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  1. K. A. Mishina
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  2. E. N. Korchagina
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  3. I. V. Kazartsev
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Correspondence to K. A. Mishina.

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Translated from Izmeritel’naya Tekhnika, No. 9, pp. 11–17, September 2023. Russian DOI: https://doi.org/10.32446/0368-1025it.2023-9-11-17

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Original article submitted 06/26/2023. Accepted 09/10/2023

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Mishina, K.A., Korchagina, E.N. & Kazartsev, I.V. GET 133-2023 State Primary Special Standard for the unit of heat in the field of solution and reaction calorimetry. Meas Tech 66, 647–655 (2023). https://doi.org/10.1007/s11018-024-02277-2

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  • DOI: https://doi.org/10.1007/s11018-024-02277-2

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