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Modulated capillary titration calorimeter

Theoretical and experimental studies

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Abstract

A modulated capillary titration calorimeter has been developed. New software and optimization of the calorimetric unit CTD2156 are used as a basis of the modulated capillary titration calorimeter. The scanning mode of the calorimeter has been theoretically substantiated. The scanning of chambers temperature is provided due to the fact that the shield temperature is linearly varied at heating and cooling. The reversing and kinetic part of the total heat flow are measured at heating of a diluted collagen solution. The main advantage of the calorimeter is its ability to operate in a modulation mode, in an isothermal mode, in modes of linear heating and cooling of homogeneous and dispersoid liquid samples at an effective mixing of reagents in calorimetric chambers.

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Authors and Affiliations

  1. Institute for Biological Instrumentation, Russian Academy of Sciences, 142290, Pushchino, Moscow Region, Russia

    G. V. Kotelnikov, S. P. Moiseyeva & E. V. Mezhburd

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  1. G. V. Kotelnikov
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  2. S. P. Moiseyeva
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  3. E. V. Mezhburd
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Correspondence to G. V. Kotelnikov.

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Kotelnikov, G.V., Moiseyeva, S.P. & Mezhburd, E.V. Modulated capillary titration calorimeter. J Therm Anal Calorim 92, 631–634 (2008). https://doi.org/10.1007/s10973-007-8718-z

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  • DOI: https://doi.org/10.1007/s10973-007-8718-z

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