Skip to main content
SpringerLink
Log in

Utilizationof dta for two-step synthesisof Cu–Mn–Cr spinel

  • regular
  • Published:
Journal of Thermal Analysis and Calorimetry Aims and scope Submit manuscript

Abstract

The novel two-step synthesis method decreasing the calcining temperature necessary for formation of spinel lattice and as well for reaching of bright and clear hue of the pigments prepared were investigated. This work aims to utilization of DTA for synthesis monitoring. Influence of raw materials and temperature of calcination on color properties were observed. The characterization of the samples was performed by X-ray diffraction and colorimetry in the CIE L*a*b* system. It was proved that the black spinel pigment Cu2.3Mn2.8Cr4.9Ox can be prepared at finally temperature 700°C as one-phase system with high quality black hue.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. M Trojan Z Šolc M Novotný et al. (1996) Pigments, Kirk-Othmer Encyclopedia of Chem. Technol., Vol. 19 John Wiley and Sons Inc. New York 45

    Google Scholar 

  2. DCMA – Classification and Chemical Description of the Mixed Metal Oxide Inorganic Colored Pigments, Metal Oxides and Ceramic Color, Subcommitte DCMA, 1982.

  3. G. Buxbaum, Industrial Inorganic Pigments, Weinheim 1993.

  4. E Ozel S Turan (2003) J. Eur. Ceram. Soc. 23 2097 Occurrence Handle10.1016/S0955-2219(03)00036-0 Occurrence Handle1:CAS:528:DC%2BD3sXktF2lu78%3D

    Article  CAS  Google Scholar 

  5. G Yang B Han Z Sun L Yan X Wang (2002) Dyes and Pigments 55 9 Occurrence Handle10.1016/S0143-7208(02)00056-6 Occurrence Handle1:CAS:528:DC%2BD38XntVWms7s%3D

    Article  CAS  Google Scholar 

  6. MP Gonzales-Sandoval AM Beesley M Miki-Yoshida (2004) J. Alloys Compd. 369 190 Occurrence Handle10.1016/j.jallcom.2003.09.101

    Article  Google Scholar 

  7. J Ponce E Rios JL Rehspringer G Poillerat (1999) J. Solid State Chem. 145 23 Occurrence Handle10.1006/jssc.1999.8162 Occurrence Handle1:CAS:528:DyaK1MXkt1ektbw%3D

    Article  CAS  Google Scholar 

  8. SC Souza IMG Santos MRS Silva MR Cassia-Santos (2005) J. Therm. Anal. Cal. 79 451 Occurrence Handle10.1007/s10973-005-0083-1 Occurrence Handle1:CAS:528:DC%2BD2MXkt1ChsLc%3D

    Article  CAS  Google Scholar 

  9. S Roy J Ghose (1999) Mater. Res. Bull. 29 1179 Occurrence Handle10.1016/S0025-5408(99)00109-9

    Article  Google Scholar 

  10. S Chemlal A Larbot M Persin J Sarrazin (2000) Mater. Res. Bull. 1 2515 Occurrence Handle10.1016/S0025-5408(00)00444-X

    Article  Google Scholar 

  11. SC Souza MAF Souza SJG Lima MR Cassia-Santos (2005) J. Therm. Anal. Cal. 79 455 Occurrence Handle10.1007/s10973-005-0084-0 Occurrence Handle1:CAS:528:DC%2BD2MXkt1Chsb4%3D

    Article  CAS  Google Scholar 

  12. Ž Mesíková P Šulcová M Trojan (2006) J. Therm. Anal. Cal. 84 733 Occurrence Handle10.1007/s10973-005-7543-5

    Article  Google Scholar 

  13. XJ Yang ES Liu NS Chen (1998) Appl. Chem. 15 14 Occurrence Handle1:CAS:528:DyaK1cXnsFGrtL4%3D

    CAS  Google Scholar 

  14. LJ Wang CL Zhang S Li (1996) J. Inorg. Chem. 12 377

    Google Scholar 

  15. Ž Mesíkova P Šulcová M Trojan (2005) Ceramics-Silikáty 49 48

    Google Scholar 

  16. M Trojan P Šulcová D Brandová (1998) J. Therm. Anal. Cal. 53 639 Occurrence Handle10.1023/A:1010178416902 Occurrence Handle1:CAS:528:DyaK1cXns1Oms7g%3D

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Inorganic Technology, Faculty of Chemical Technology, University of Pardubice, Pardubice, Czech Republic, 532 10, nám. Čs. legií 565

    P. Bělina & Petra Šulcová

Authors
  1. P. Bělina
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Petra Šulcová
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to P. Bělina.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Bělina, P., Šulcová, P. Utilizationof dta for two-step synthesisof Cu–Mn–Cr spinel. J Therm Anal Calorim 88, 107–110 (2007). https://doi.org/10.1007/s10973-006-8100-6

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10973-006-8100-6

Keywords

Search

Navigation