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Copper(II) acetates with aliphatic/heterocyclic amines

Coupled TG-DTA-EGA study, IR characterization and structure correlation

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Summary

Three copper acetate complex compounds, namely Cu(CH3COO)2(en)2·2H2O (I), Cu(CH3COO)2(tn)2(II) and Cu2(CH3COO)4(pyz) (III) (en=ethylenediamine, tn=1,3-diaminopropane, pyz=pyrazine), were prepared and characterized during heating in argon by thermogravimetry (TG), differential thermal analysis (DTA) and evolved gas analysis (EGA) using mass spectrometry (MS). The results of infrared spectroscopy (IR) were evaluated to be used as a spectroscopic criterion for the determination of the carboxylate binding mode in the compounds.

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Authors and Affiliations

  1. Institute of Chemical Science, Faculty of Sciences, P. J. Šafárik University, Moyzesova 11, 041 54 Košice, Slovak Republic

    V. ZeleÔák

  2. Institute of Chemical Science, Faculty of Sciences, P. J. Šafárik University, Moyzesova 11, 041 54 Košice, Slovak Republic

    Z. Vargová

  3. Institute of Chemical Science, Faculty of Sciences, P. J. Šafárik University, Moyzesova 11, 041 54 Košice, Slovak Republic

    Katalin Györyová

  4. Institute of Inorganic Chemistry, AS CR, 250 68 Rež, Czech Republic

    E. Ve?erníková

  5. Nuclear Research Institute, 250 68 Rež, Czech Republic

    V. Balek

Authors
  1. V. ZeleÔák
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  2. Z. Vargová
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  3. Katalin Györyová
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  4. E. Ve?erníková
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  5. V. Balek
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ZeleÔák, V., Vargová, Z., Györyová, K. et al. Copper(II) acetates with aliphatic/heterocyclic amines. J Therm Anal Calorim 82, 747–754 (2005). https://doi.org/10.1007/s10973-005-0959-0

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  • DOI: https://doi.org/10.1007/s10973-005-0959-0

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