Abstract
PTA (peroxo titanic acid) gel was prepared by a modified sol-gel method from peroxo titanic acid using TiCl4/ethanol/water solution as the starting material at room temperature. Physicochemical properties of heat-treated gel were characterized by IR, XRD, TG-DTA and SEM. Optimal preparing conditions were chosen to prepare anatase film for the photocatalytic degradation of methyl orange. The dip-coating technique was used to synthesis the supported anatase film on quartz glass. Photocatalytic efficiency for the degradation of methyl orange under UV irradiation was also examined. It was found that the degradation efficiency of the anatase film synthesized in this paper is higher than commercial titania P25.
Similar content being viewed by others
References
Dillert R, Cassano AE, Goslich R, Bahnemann D (1999) Catal Today 54:267
Robert D, Malato S (2002) Sci Total Environ 291:85
Lindner M, Bahnemann DW, Hirthe B, Griebler W (1995) Solar Eng 1:399
Herrmann JM (1999) Catal Today 53:115
Lee SK, Mills A (2004) J Ind Eng Chem 10:173
Bahnemann D (2004) Solar Energy 77:445
Pichat P, Disdier J, Hoang-Van C, Mas D, Goutailler G, Gaysse C (2000) Catal Today 63:363
Peral J, Domenech X, Ollis DF (1997) J Chem Technol Biotechnol 70:117
Mills A, Le Hunte S (1997) J Photochem Photobiol A 108:1
Lindner M, Theurich J, Bahnemann D (1997) Water Sci Technol 35:79
Brandi RJ, Martin CA, Alfano OM, Cassano AE (2002) J Adv Oxid Technol 5:175
Ding Z, Hu X, Yue PL, Lu GQ (2001) Catal Today 68:173
Kaitvichyanukul P, Chenthamarakshan CR, Rajeshwar K, Qasim SR (2002) J Electroanal Chem 519:25
Dislich H, Hussman E (1981) Thin Solid Films 77:129
Smirnova N, Eremenko A, Rusina O (2001) J Sol-Gel Sci Technol 22:109
Kamiya K, Tanimoto K, Yoko T (1986) J Mater Sci Lett 5:402
Yoldas BE (1986) J Mater Sci 21:1087
Ichinose H, Terasaki M, Katsuki H (1996) J Ceramic Soc Jpn 104:715
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Yuan, Z., Li, B., Zhang, J. et al. Synthesis of TiO2 thin film by a modified sol-gel method and properties of the prepared films for photocatalyst. J Sol-Gel Sci Technol 39, 249–253 (2006). https://doi.org/10.1007/s10971-006-8164-6
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s10971-006-8164-6