Skip to main content
Log in

Ion Irradiation–Induced Modification of Electrical Properties of YBa2Cu3O7-x NanoSQUIDs

  • Original Paper
  • Published:
Journal of Superconductivity and Novel Magnetism Aims and scope Submit manuscript

Abstract

We report on the fabrication and characterization of nanopatterned superconducting quantum interference devices (SQUIDs) based on bi-crystal MgO with 24° misorientation angle in epitaxially grown YBa2Cu3O7−δ thin films. Nanopatterning is performed by Ga+ focused ion beam milling. We present a study of the effect of ion irradiation–induced modification of electrical properties of YBa2Cu3O7−δ nanoSQUIDs to uncover the performance of the nanoSQUIDs without Au as shunting layer, which have potential to reduce the intrinsic thermal flux noise. In this experiment, seven YBCO nanoSQUIDs are fabricated and measured under liquid helium temperature. The statistical results of I–V characteristics illustrate that the properties of YBCO nanoSQUIDs without Au as protection layer are sensitive to ion beam irradiation during focused ion beam (FIB) cutting process. As a consequence, the critical current Ic changes between 10.3 and 107 μA with resistance 120 Ω and 16.5 Ω respectively. In other words, the SQUID voltage is almost stable. Surprisingly, none of them shows hysteresis I–V characteristics even the resistance up to 120 Ω, which is not the case for YBa2Cu3O7−δ nanoSQUIDs based on SrTiO3 bi-crystal. In view of above-mentioned, we propose to deposit one insulating layer as protection layer around grain boundary of MgO to avoid the degradation of critical current and increase the resistance.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8

Similar content being viewed by others

Data Availability

The data that support the findings of this study are available within the article and its supplementary material.

References

  1. Likharev, K.K.: Superconducting weak links. Rev. Mod. Phys. 51(1), 101 (1979)

    Article  ADS  Google Scholar 

  2. Koelle, D., Kleiner, R., Ludwig, F., Dantsker, E., Clarke, J.: High-transition temperature superconducting quantum interference devices. Rev. Mod. Phys. 71(3), 631 (1999)

    Article  ADS  Google Scholar 

  3. Hilgenkamp, H., Mannhart, J.: Grain boundaries in high-Tc superconductors. Rev. Mod. Phys. 74(2), 485 (2002)

    Article  ADS  Google Scholar 

  4. Granata, C., Vettoliere, A.: Nano superconducting quantum interference device: a powerful tool for nanoscale investigations. Phys. Rep. 614, 1–69 (2016)

    Article  ADS  MathSciNet  Google Scholar 

  5. Gallop, J., Hao, L.: Nanoscale superconducting quantum interference devices add another dimension. ACS Nano 10(9), 8128–8132 (2016)

    Article  Google Scholar 

  6. Everitt, M.J., Clark, T.D., Stiffell, P.B., Vourdas, A., Ralph, J.F., Prance, R.J., Prance, H.: Superconducting analogs of quantum optical phenomena: macroscopic quantum superpositions and squeezing in a superconducting quantum-interference device ring. Phys. Rev. A 69(4), 043804 (2004)

    Article  ADS  Google Scholar 

  7. Wölbing, R., Schwarz, T., Müller, B., Nagel, J., Kemmler, M., Kleiner, R., Koelle, D.: Optimizing the spin sensitivity of grain boundary junction nanoSQUIDs-towards detection of small spin systems with single-spin resolution. Supercond. Sci. Technol. 27(12), 125007 (2014)

    Article  ADS  Google Scholar 

  8. Schäfer-Nolte, E., Schlipf, L., Ternes, M., Reinhard, F., Kern, K., Wrachtrup, J.: Tracking temperature-dependent relaxation times of ferritin nanomagnets with a wideband quantum spectrometer. Phys. Rev. Lett. 113(21), 217204 (2014)

    Article  ADS  Google Scholar 

  9. Ganzhorn, M., Klyatskaya, S., Ruben, M., Wernsdorfer, W.: Carbon nanotube nanoelectromechanical systems as magnetometers for single-molecule magnets. ACS Nano 7(7), 6225–6236 (2013)

    Article  Google Scholar 

  10. Lipert, K., Bahr, S., Wolny, F., Atkinson, P., Weißker, U., Mühl, T., Klingeler, R.: An individual iron nanowire-filled carbon nanotube probed by micro-Hall magnetometry. Appl. Phys. Lett. 97(21), 212503 (2010)

    Article  ADS  Google Scholar 

  11. Wernsdorfer, W.: Classical and quantum magnetization reversal studied in nanometer-sized particles and clusters. Handb. Adv. Magn. Mater. 77–127 (2006)

  12. Nagel, J., Konovalenko, K.B., Kemmler, M., Turad, M., Werner, R., Kleisz, E., Koelle, D.: Resistively shunted YBa2Cu3O7 grain boundary junctions and low-noise SQUIDs patterned by a focused ion beam down to 80 nm linewidth. Supercond. Sci. Technol. 24(1), 015015 (2010)

    Article  ADS  Google Scholar 

  13. Schwarz, T., Wölbing, R., Reiche, C.F., Müller, B., Martínez-Pérez, M.J., Mühl, T., Koelle, D.: Low-noise YBa2Cu3O7 nano-SQUIDs for performing magnetization-reversal measurements on magnetic nanoparticles. Phys. Rev. Appl. 3(4), 044011 (2015)

    Article  ADS  Google Scholar 

  14. Lin, J., Müller, B., Linek, J., Karrer, M., Wenzel, M., Martínez-Pérez, M.J., Koelle, D.: YBa2Cu3O7 nano superconducting quantum interference devices on MgO bicrystal substrates. Nanoscale 12(9), 5658–5668 (2020)

    Article  Google Scholar 

  15. Civale, L., Marwick, A.D., McElfresh, M.W., Worthington, T.K., Malozemoff, A.P., Holtzberg, F.H., Kirk, M.A.: Defect independence of the irreversibility line in proton-irradiated Y-Ba-Cu-O crystals. Phys. Rev. Lett. 65(9), 1164 (1990)

    Article  ADS  Google Scholar 

  16. Civale, L., Marwick, A.D., Worthington, T.K., Kirk, M.A., Thompson, J.R., Krusin-Elbaum, L., Holtzberg, F.: Vortex confinement by columnar defects in YBa2Cu3O7 crystals: enhanced pinning at high fields and temperatures. Phys. Rev. Lett. 67(5), 648 (1991)

    Article  ADS  Google Scholar 

  17. Krusin‐Elbaum, L., Thompson, J.R., Wheeler, R., Marwick, A.D., Li, C., Patel, S., ... Ullmann, J.: Enhancement of persistent currents in Bi2Sr2CaCu2O8 tapes with splayed columnar defects induced with 0.8 GeV protons. Appl. Phys. Lett. 64(24), 3331–3333 (1994)

  18. Shani, L., Fried, A., Fleger, Y., Girshevitz, O., Sharoni, A., Yeshurun, Y.: Effect of focused ion beam irradiation on superconducting nanowires. J. Supercond. Nov. Magn. 1–5 (2022)

  19. Roas, B., Hensel, B., Saemann-Ischenko, G., Schultz, L.: Irradiation-induced enhancement of the critical current density of epitaxial YBa2Cu3O7-x thin films. Appl. Phys. Lett. 54(11), 1051–1053 (1989)

    Article  ADS  Google Scholar 

  20. Sefrioui, Z., Arias, D., Gonzalez, E.M., Leon, C., Santamaria, J., Vicent, J.L.: Vortex liquid entanglement in irradiated YBa2Cu3O7 thin films. Phys. Rev. B 63(6), 064503 (2001)

    Article  ADS  Google Scholar 

  21. Wu, J.Z., Yu, N., Chu, W.K.: Anisotropy of the ion-beam radiation effect in YBa2Cu3O7-δ (110) thin films. Phys. Rev. B 48(13), 9929 (1993)

    Article  ADS  Google Scholar 

  22. Drung, D., Mück, M: The SQUID Handbook vol I ed J Clarke and AI Braginski. (2004)

  23. Foglietti, V.: Double dc SQUID for flux-locked-loop operation. Appl. Phys. Lett. 59(4), 476–478 (1991)

    Article  ADS  Google Scholar 

  24. Stewart, W.C.: Current-voltage characteristics of Josephson junctions. Appl. Phys. Lett. 12(8), 277–280 (1968)

    Article  ADS  Google Scholar 

  25. McCumber, D.E.: Effect of ac impedance on dc voltage-current characteristics of superconductor weak-link junctions. J. Appl. Phys. 39(7), 3113–3118 (1968)

    Article  ADS  Google Scholar 

  26. Jorgensen, J.D., Beno, M.A., Hinks, D.G., Soderholm, L., Volin, K.J., Hitterman, R.L., Grace, J.D., Schuller, C.U., Segre, I.K., Zhang, K., Kleefisch, M.S.: Oxygen ordering and the orthorhombic-to-tetragonal phase transition in YBa2Cu3O7-x. Phys. Rev. B 36(7), 3608 (1987)

    Article  ADS  Google Scholar 

  27. Jorgensen, J.D., Veal, B.W., Paulikas, A.P., Nowicki, L.J., Crabtree, G.W., Claus, H., Kwok, W.K.: Structural properties of oxygen-deficient YBa2Cu3O7-δ. Phys. Rev. B 41(4), 1863 (1990)

    Article  ADS  Google Scholar 

  28. Daeumling, M., Seuntjens, J.M., Larbalestier, D.C.: Oxygen-defect flux pinning, anomalous magnetization and intra-grain granularity in YBa2Cu307-δ. Nature 346(6282), 332–335 (1990)

    Article  ADS  Google Scholar 

  29. Chen, C.H., White, A.E., Short, K.T., Dynes, R.C., Poate, J.M., Jacobson, D.C., Howard, R.E.: Ion beam induced damage and superlattice formation in epitaxial YBa2Cu3O7-δ thin films. Appl. Phys. Lett. 54(12), 1178–1180 (1989)

    Article  ADS  Google Scholar 

Download references

Acknowledgements

We gratefully acknowledge fruitful discussions and technical support by M. Turad, R. Löffler (LISA +), D. Kölle, and R. Kleiner and by C. Back.

Funding

This work was supported by the COST action NANOCOHYBRI (CA16218), the National Natural Science Foundation of China (12104112), and the Natural Science Foundation of Shandong Province (ZR2021QA036).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to JianXin Lin.

Ethics declarations

Competing Interests

The authors declare no competing interests.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Lin, J., Wang, Q., Zhang, D. et al. Ion Irradiation–Induced Modification of Electrical Properties of YBa2Cu3O7-x NanoSQUIDs. J Supercond Nov Magn 35, 2671–2677 (2022). https://doi.org/10.1007/s10948-022-06306-5

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10948-022-06306-5

Keywords

Navigation