Abstract
We report on the fabrication and characterization of nanopatterned superconducting quantum interference devices (SQUIDs) based on bi-crystal MgO with 24° misorientation angle in epitaxially grown YBa2Cu3O7−δ thin films. Nanopatterning is performed by Ga+ focused ion beam milling. We present a study of the effect of ion irradiation–induced modification of electrical properties of YBa2Cu3O7−δ nanoSQUIDs to uncover the performance of the nanoSQUIDs without Au as shunting layer, which have potential to reduce the intrinsic thermal flux noise. In this experiment, seven YBCO nanoSQUIDs are fabricated and measured under liquid helium temperature. The statistical results of I–V characteristics illustrate that the properties of YBCO nanoSQUIDs without Au as protection layer are sensitive to ion beam irradiation during focused ion beam (FIB) cutting process. As a consequence, the critical current Ic changes between 10.3 and 107 μA with resistance 120 Ω and 16.5 Ω respectively. In other words, the SQUID voltage is almost stable. Surprisingly, none of them shows hysteresis I–V characteristics even the resistance up to 120 Ω, which is not the case for YBa2Cu3O7−δ nanoSQUIDs based on SrTiO3 bi-crystal. In view of above-mentioned, we propose to deposit one insulating layer as protection layer around grain boundary of MgO to avoid the degradation of critical current and increase the resistance.
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References
Likharev, K.K.: Superconducting weak links. Rev. Mod. Phys. 51(1), 101 (1979)
Koelle, D., Kleiner, R., Ludwig, F., Dantsker, E., Clarke, J.: High-transition temperature superconducting quantum interference devices. Rev. Mod. Phys. 71(3), 631 (1999)
Hilgenkamp, H., Mannhart, J.: Grain boundaries in high-Tc superconductors. Rev. Mod. Phys. 74(2), 485 (2002)
Granata, C., Vettoliere, A.: Nano superconducting quantum interference device: a powerful tool for nanoscale investigations. Phys. Rep. 614, 1–69 (2016)
Gallop, J., Hao, L.: Nanoscale superconducting quantum interference devices add another dimension. ACS Nano 10(9), 8128–8132 (2016)
Everitt, M.J., Clark, T.D., Stiffell, P.B., Vourdas, A., Ralph, J.F., Prance, R.J., Prance, H.: Superconducting analogs of quantum optical phenomena: macroscopic quantum superpositions and squeezing in a superconducting quantum-interference device ring. Phys. Rev. A 69(4), 043804 (2004)
Wölbing, R., Schwarz, T., Müller, B., Nagel, J., Kemmler, M., Kleiner, R., Koelle, D.: Optimizing the spin sensitivity of grain boundary junction nanoSQUIDs-towards detection of small spin systems with single-spin resolution. Supercond. Sci. Technol. 27(12), 125007 (2014)
Schäfer-Nolte, E., Schlipf, L., Ternes, M., Reinhard, F., Kern, K., Wrachtrup, J.: Tracking temperature-dependent relaxation times of ferritin nanomagnets with a wideband quantum spectrometer. Phys. Rev. Lett. 113(21), 217204 (2014)
Ganzhorn, M., Klyatskaya, S., Ruben, M., Wernsdorfer, W.: Carbon nanotube nanoelectromechanical systems as magnetometers for single-molecule magnets. ACS Nano 7(7), 6225–6236 (2013)
Lipert, K., Bahr, S., Wolny, F., Atkinson, P., Weißker, U., Mühl, T., Klingeler, R.: An individual iron nanowire-filled carbon nanotube probed by micro-Hall magnetometry. Appl. Phys. Lett. 97(21), 212503 (2010)
Wernsdorfer, W.: Classical and quantum magnetization reversal studied in nanometer-sized particles and clusters. Handb. Adv. Magn. Mater. 77–127 (2006)
Nagel, J., Konovalenko, K.B., Kemmler, M., Turad, M., Werner, R., Kleisz, E., Koelle, D.: Resistively shunted YBa2Cu3O7 grain boundary junctions and low-noise SQUIDs patterned by a focused ion beam down to 80 nm linewidth. Supercond. Sci. Technol. 24(1), 015015 (2010)
Schwarz, T., Wölbing, R., Reiche, C.F., Müller, B., Martínez-Pérez, M.J., Mühl, T., Koelle, D.: Low-noise YBa2Cu3O7 nano-SQUIDs for performing magnetization-reversal measurements on magnetic nanoparticles. Phys. Rev. Appl. 3(4), 044011 (2015)
Lin, J., Müller, B., Linek, J., Karrer, M., Wenzel, M., Martínez-Pérez, M.J., Koelle, D.: YBa2Cu3O7 nano superconducting quantum interference devices on MgO bicrystal substrates. Nanoscale 12(9), 5658–5668 (2020)
Civale, L., Marwick, A.D., McElfresh, M.W., Worthington, T.K., Malozemoff, A.P., Holtzberg, F.H., Kirk, M.A.: Defect independence of the irreversibility line in proton-irradiated Y-Ba-Cu-O crystals. Phys. Rev. Lett. 65(9), 1164 (1990)
Civale, L., Marwick, A.D., Worthington, T.K., Kirk, M.A., Thompson, J.R., Krusin-Elbaum, L., Holtzberg, F.: Vortex confinement by columnar defects in YBa2Cu3O7 crystals: enhanced pinning at high fields and temperatures. Phys. Rev. Lett. 67(5), 648 (1991)
Krusin‐Elbaum, L., Thompson, J.R., Wheeler, R., Marwick, A.D., Li, C., Patel, S., ... Ullmann, J.: Enhancement of persistent currents in Bi2Sr2CaCu2O8 tapes with splayed columnar defects induced with 0.8 GeV protons. Appl. Phys. Lett. 64(24), 3331–3333 (1994)
Shani, L., Fried, A., Fleger, Y., Girshevitz, O., Sharoni, A., Yeshurun, Y.: Effect of focused ion beam irradiation on superconducting nanowires. J. Supercond. Nov. Magn. 1–5 (2022)
Roas, B., Hensel, B., Saemann-Ischenko, G., Schultz, L.: Irradiation-induced enhancement of the critical current density of epitaxial YBa2Cu3O7-x thin films. Appl. Phys. Lett. 54(11), 1051–1053 (1989)
Sefrioui, Z., Arias, D., Gonzalez, E.M., Leon, C., Santamaria, J., Vicent, J.L.: Vortex liquid entanglement in irradiated YBa2Cu3O7 thin films. Phys. Rev. B 63(6), 064503 (2001)
Wu, J.Z., Yu, N., Chu, W.K.: Anisotropy of the ion-beam radiation effect in YBa2Cu3O7-δ (110) thin films. Phys. Rev. B 48(13), 9929 (1993)
Drung, D., Mück, M: The SQUID Handbook vol I ed J Clarke and AI Braginski. (2004)
Foglietti, V.: Double dc SQUID for flux-locked-loop operation. Appl. Phys. Lett. 59(4), 476–478 (1991)
Stewart, W.C.: Current-voltage characteristics of Josephson junctions. Appl. Phys. Lett. 12(8), 277–280 (1968)
McCumber, D.E.: Effect of ac impedance on dc voltage-current characteristics of superconductor weak-link junctions. J. Appl. Phys. 39(7), 3113–3118 (1968)
Jorgensen, J.D., Beno, M.A., Hinks, D.G., Soderholm, L., Volin, K.J., Hitterman, R.L., Grace, J.D., Schuller, C.U., Segre, I.K., Zhang, K., Kleefisch, M.S.: Oxygen ordering and the orthorhombic-to-tetragonal phase transition in YBa2Cu3O7-x. Phys. Rev. B 36(7), 3608 (1987)
Jorgensen, J.D., Veal, B.W., Paulikas, A.P., Nowicki, L.J., Crabtree, G.W., Claus, H., Kwok, W.K.: Structural properties of oxygen-deficient YBa2Cu3O7-δ. Phys. Rev. B 41(4), 1863 (1990)
Daeumling, M., Seuntjens, J.M., Larbalestier, D.C.: Oxygen-defect flux pinning, anomalous magnetization and intra-grain granularity in YBa2Cu307-δ. Nature 346(6282), 332–335 (1990)
Chen, C.H., White, A.E., Short, K.T., Dynes, R.C., Poate, J.M., Jacobson, D.C., Howard, R.E.: Ion beam induced damage and superlattice formation in epitaxial YBa2Cu3O7-δ thin films. Appl. Phys. Lett. 54(12), 1178–1180 (1989)
Acknowledgements
We gratefully acknowledge fruitful discussions and technical support by M. Turad, R. Löffler (LISA +), D. Kölle, and R. Kleiner and by C. Back.
Funding
This work was supported by the COST action NANOCOHYBRI (CA16218), the National Natural Science Foundation of China (12104112), and the Natural Science Foundation of Shandong Province (ZR2021QA036).
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Lin, J., Wang, Q., Zhang, D. et al. Ion Irradiation–Induced Modification of Electrical Properties of YBa2Cu3O7-x NanoSQUIDs. J Supercond Nov Magn 35, 2671–2677 (2022). https://doi.org/10.1007/s10948-022-06306-5
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DOI: https://doi.org/10.1007/s10948-022-06306-5