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Size Controlled Synthesis of CoFe2O4 Nanoparticles with Polyethylene Glycol

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Abstract

Nanoparticles (NPs) of CoFe2O4, which is a well-known spinel ferrite and hard magnetic material with very high cubic magnetocrystalline anisotropy, were synthesized by co-precipitation method. The effect of different molecular weights of polyethyleneglycol (PEG) on the magnetic properties and crystallite size of CoFe2O4 NPs was investigated by using PEG-400, PEG-10.000 and, PEG-20.000. Crystalline structure and size of CoFe2O4 NPs were studied using X-ray diffraction (XRD). The VSM studies showed that the saturation magnetization (M s ) and coercivity (H c ) of the CoFe2O4 NPs depend on molecular weight of PEG.

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References

  1. Miller, M.M., Prinz, G.A., Cheng, S.F., Bounnak, S.: Appl. Phys. Lett. 81, 2211 (2002)

    Article  ADS  Google Scholar 

  2. Sun, S., Murray, C.B., Weller, D., Folks, L., Moser, A.: Science 287, 1989 (2000)

    Article  ADS  Google Scholar 

  3. Caruso, F., Spasova, M., Susha, A., Giersig, M., Caruso, R.A.: Chem. Mater. 13, 109 (2001)

    Article  Google Scholar 

  4. Hyeon, T., Chung, Y., Park, J., Lee, S.S., Kim, Y.W., Park, B.H.: J. Phys. Chem. B 106, 6831 (2002)

    Article  Google Scholar 

  5. Wang, J., Deng, T., Lin, Y., Yang, C., Zhan, W.: J. Alloys Compd. 450, 532 (2008)

    Article  Google Scholar 

  6. Petcharoen, K., Sirivat, A.: Mater. Sci. Eng. B, Solid-State Mater. Adv. Technol. 177, 421 (2012)

    Article  Google Scholar 

  7. Maaz, K., Karim, S., Mumtaz, A., Hasanain, S.K., Liu, J., Duan, J.L.: J. Magn. Magn. Mater. 321, 1838 (2009)

    Article  ADS  Google Scholar 

  8. Madani, S.S., Mahmoudzadeh, G., Khorrami, S.A.: J. Ceram Process. Res. 13, 123 (2012)

    Google Scholar 

  9. Shen, L., Qiao, Y., Guo, Y., Meng, S., Yang, G., Wu, M., Zhao, J.: Ceram. Int. 40, 1519 (2014)

    Article  Google Scholar 

  10. Topkaya, R., Kurtan, U., Baykal, A., Sözeri, H., Toprak, M.S.: J. Inorg. Organomet. Polym. 23, 592 (2013)

    Article  Google Scholar 

  11. Kato, K., Tsuge, A., Niihara, K.: J. Am. Ceram. Soc. 79, 1483 (1996)

    Article  Google Scholar 

  12. Aziz, M., Abbas, S., Rosemaria, W., Baharom, W.: Mater. Lett. 91, 31 (2013)

    Article  Google Scholar 

  13. Kasapoğlu, N., Baykal, A., Köseoğlu, Y., Toprak, M.S.: Scr. Mater. 57, 441 (2007)

    Article  Google Scholar 

  14. Wejrzanowski, T., Pielaszek, R., Opalinska, A., Matysiak, H., Łojkowski, W., Kurzydłowski, K.J.: Appl. Surf. Sci. 253, 204 (2006)

    Article  ADS  Google Scholar 

  15. Kumar, S.R., et al.: Surfactant-free solvothermal synthesis of monodispersed 3D hierarchical Fe3O4 microspheres. Mater. Lett. (2013). doi:10.1016/j.matlet.2013.08.005

    Google Scholar 

  16. Waldron, R.D.: Phys. Rev. 99, 1727 (1955)

    Article  ADS  Google Scholar 

  17. Singhal, S., Singh, J., Barthwal, S.K., Chandra, K.: J. Solid State Chem. 178, 3183 (2005)

    Article  ADS  Google Scholar 

  18. Phadatare, M.R., Khot, V.M., Salunkhe, A.B., Thorat, N.D., Pawar, S.H.: J. Magn. Magn. Mater. 324, 770 (2012)

    Article  ADS  Google Scholar 

  19. Bricenoa, S., Escamilla, W.B., Silva, P., Delgado, G.E., Plaza, E., Palacios, J., Canizales, E.: J. Magn. Magn. Mater. 324, 2926 (2012)

    Article  ADS  Google Scholar 

  20. Kurtan, U., Topkaya, R., Baykal, A.: Mater. Res. Bull. 48, 4889 (2013)

    Article  Google Scholar 

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Acknowledgements

This work is supported by Fatih University under BAP grant No. P50021203-Y (2282).

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Authors and Affiliations

  1. Department of Chemistry, Fatih University, 34500, B.Çekmece-Istanbul, Turkey

    S. Esir & A. Baykal

  2. TUBITAK-UME, National Metrology Institute, P.O. Box 54, 41470, Gebze-Kocaeli, Turkey

    H. Sözeri

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  1. S. Esir
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  2. A. Baykal
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  3. H. Sözeri
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Correspondence to A. Baykal.

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Esir, S., Baykal, A. & Sözeri, H. Size Controlled Synthesis of CoFe2O4 Nanoparticles with Polyethylene Glycol. J Supercond Nov Magn 27, 1309–1313 (2014). https://doi.org/10.1007/s10948-013-2446-3

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  • DOI: https://doi.org/10.1007/s10948-013-2446-3

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