Abstract
The results of studies on the structure of organic complexes of the derivatives of 1,3-dihydropyrimidine-2,4-diones and their structural analogues with macrocyclic poly- and azapolyethers are generalized.
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(a) E. A. Meyer, R. K. Castellano, and F. Diederich, Angew. Chem. Int. Ed., 42, 1210–1250 (2003); (b) S. Tsuzuki, K. Dhonda, T. Uchimaru, et al., J. Am. Chem. Soc., 124, 104–112 (2002); (c) G. R. Desiraju and T. Steiner, The Weak Hydrogen Bond in Structural Chemistry and Biology, Oxford University Press, Oxford (1999), pp. 29–121.
(a) M. Gallant, M. T. P. Viet, and J. D. Wuest, J. Am. Chem. Soc., 113, 721–723 (1991); (b) J. A. Zerkowski, C. T. Seto, and G. M. Whitesides, ibid., 114, 5473–5475 (1992); (c) E. Boucher, M. Simard, and J. D. Wuest, J. Org. Chem., 60, 1408–1412 (1995); (d) H. Chen, Meena, and L. W. McLaughlin, J. Am. Chem. Soc., 130, 13190/13191 (2008); (e) W. C. Drewe and S. Neidle, Chem. Comm., 5295–5297 (2008).
(a) Y. Liu, Y.-W. Yang, L. Li, and Y. Chen, Org. Biomol. Chem., 2, 1542–1548 (2004); (b) S.-K. Chang, D. Van Engen, E. Fan, and A. D. Hamilton, J. Am. Chem. Soc., 113, 7640–7645 (1991).
(a) A. Elbasyouny, H. J. Brugge, K. Deuten, et al., ibid., 105, 6568–6577 (1983); (b) Yu. A. Simonv, M. S. Fonari, A. A. Dvorkin, and T. I. Malinovskii, Structural Crystallography [in Russian], To 100th anniversary of Academician N. V. Belov’s birth, Nauka, Moscow (1992), pp. 221–250.
Y. A. Simonov, M. S. Fonari, M. J. Zaworotko, et al., Org. Biomol. Chem., 1, 2922–2929 (2003).
M. S. Fonari, Y. A. Simonov, W.-J. Wang, et al., CrystEngComm., 11, 94–101 (2009).
(a) A. D. Burrows, M. P. Mingos, A. J. P. White, and D. J. Williams, J. Chem. Soc. Dalton Trans., 3805–3812 (1996); (b) S. Aoki, M. Shiro, T. Koike, and E. Kimura, J. Am. Chem. Soc., 122, 576–584 (2000); (c) G. S. Papaefstathiou, S. Manessi, C. P. Raptopoulou, et al., Inorg. Chem. Commun., 7, 69–72 (2004); (d) J. T. Davis and G. P. Spada, Chem. Soc. Rev., 36, 296–313 (2007); (e) J. L. Sessler, C. M. Lawrence, and J. Jayawickramarajah, ibid., 314–325.
(a) H. Rostkowska, K. Szczepaniak, M. J. Nowak, et al., J. Am. Chem. Soc., 112, 2147–2160 (1990); (b) J. Leszczynski and K. Lammertsma, J. Phys. Chem., 95, 3128–3132 (1991); (c) A. Leš and L. Adamowicz, J. Am. Chem. Soc., 112, 1504–1509 (1990); (d) H. Yekeler, J. Comp.-Aided Molec. Design., 14, 243–250 (2000); (e) H. Wang, F. Meng, W. Xu, and C. Liu, J. Mol. Struct. (Theochem.), 716, 137–141 (2005); (f) Z. Yang and M. T. Rodgers, J. Phys. Chem., A110, No. 4, 1455–1468 (2006).
W. Zielenkiewicz, Pure Appl. Chem., 71, No. 7, 1285–1290 (1999).
(a) E. Shefter and H. G. Mautner, J. Am. Chem. Soc., 89, 1249–1253 (1967); (b) E. R. T. Tiekink, Z. Kristallogr., 187, 79–84 (1989).
W.-J. Wang, E. V. Ganin, M. S. Fonari, et al., Org. Biomol. Chem., 3, 3054–3058 (2005).
(a) E. V. Ganin, M. S. Fonari, Yu. A. Simonov, et al., J. Incl. Phenom. Macrocycl. Chem., 52, 63–74 (2005); (b) M. S. Fonari, Yu. A. Simonov, G. Bocelli, et al., ibid., 61, 367–375 (2008).
Y. A. Simonov, M. S. Fonari, J. Lipkowski, et al., ibid., 46, Nos. 1/2, 27–35 (2003).
Collection of Experimental Data Obtained on a CCD Bruker Diffractometer from the Only One Thin Layered Crystal Suitable for Measurements with Linear Dimensions of 0.06×0.14×0.21 mm. C20H32N12O10 M=600.58, triclinic, P-1 space group, a=7.3954(3), b=9.7519(4), c=10.5260(5) Å, α=71.91(3), β= 78.07(2), γ=67.80(2)°, V=664.7(14) Å3, Z=1, D c=1.500 g·cms-3, μ=0.122 mms-1. The Number of Independent Reflections 1956, the Number of Reflections with [I>2σ(I)] 763, Refinement Quality 0.995, Final R Factor for [I>2σ(I)] R 1=0.1122, wR 2=0.2090. Cif-file was Deposited with the Cambridge Structural Database, No. CCDC 710152.
M. S. Fonari, Y. A. Simonov, Y. M. Chumakov, et al., Supramolec. Chem., 16, No. 1, 23–30 (2004).
M. S. Fonari, Y. A. Simonov, Y. M. Chumakov, et al., J. Struct. Chem., 46, Supplement, S96–S102 (2005).
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Original Russian Text Copyright © 2009 by Yu. A. Simonov, M. S. Fonari, J. Lipkowski, È. V. Ganin, A. A. Yavolovskii, and G. L. Kamalov
Translated from Zhurnal Strukturnoi Khimii, Vol. 50, Supplement, pp. S143–S149, 2009.
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Simonov, Y.A., Fonari, M.S., Lipkowski, J. et al. Structural features of derivatives of 1,3- dihydropyrimidine- 2,4- diones in complexes with macrocyclic poly- and azapolyethers. J Struct Chem 50 (Suppl 1), 136–142 (2009). https://doi.org/10.1007/s10947-009-0201-1
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DOI: https://doi.org/10.1007/s10947-009-0201-1