Fine-Tuning and Verification of the Experimental Set-Up
In order to see the effect of air gap length between the speaker and the specimen, a cement concrete specimen of similar geometry to the asphalt concrete specimen is used to take measurements at room temperature. Cement concrete is chosen for this particular test since its elastic behavior makes it more convenient to adjust the air gap at room temperature. Figure 4 shows that there is no significant difference in resonant frequencies due to differences in air gap lengths, except at the shortest length (20 mm) considered where there is a slight deviation (13 Hz). This also means that the effect of air resonance does not affect the measurement results at the lengths shown in Fig. 4, since there is no major difference in the amplitudes. It can also be noted that only a decrease in amplitude can be evident at longer lengths. Based on these results, it is satisfactory to adjust the air gap to one of the closest distances in Fig. 4. For the measurements taken on the actual asphalt concrete specimen, an air gap length of 40 mm is chosen based on the above findings.
A similar measurement is also taken using an impact hammer to excite the axially symmetric fundamental mode of the cement concrete specimen. This helps verify that the frequency sweep of the loudspeaker goes through the fundamental axially symmetric mode of resonance of the specimen. Figure 5 illustrates that the non-contact method measures the resonant frequency of the same mode as the impact hammer method does. By varying the amplitudes of the sound signals, the possible effect of sound intensity is monitored as shown in Fig. 5b. Even though no major differences are encountered by varying sound intensity (amplitudes), it can be noted that there are slight shifts in resonant frequencies with increase in amplitudes. These slight shifts are smaller than 0.1% in resonant frequencies and can be a manifestation of non-linearity behavior that is associated with a possible presence of discontinuity or flaw in the specimen. These slight shifts are also observed in the results from the impact hammer test (Fig. 5a).
To further illustrate the advantage of the proposed non-contact measurement setup over a similar measurement method using an impact hammer, two more measurements are performed on the asphalt concrete specimen at two measurement temperatures. The first measurement was taken 5 s after opening the thermal chamber and the second measurement was taken after 10 s. Figure 6 shows examples of comparisons at − 20 °C (Fig. 6a) and − 30 °C (Fig. 6b).
The results obtained using the impact hammer have lower measured resonant frequencies, since opening the temperature chamber disturbs the conditioning temperature. This effect is more pronounced at − 30 °C than at − 20 °C, since lower temperatures are even more sensitive to thermal disturbances by room temperature (~ 22 °C). The amount of time needed to take the measurement when using the impact hammer while the chamber is kept open has a significant effect on the results of the measurements at low temperatures.
The technique also helps to save good amount of time when there is a need to take repeated resonant frequency measurements at multiple low temperatures since it avoids the waiting time until temperature of specimens reaches the required value after its increase due to an opening of climate chambers, which is the case if we use manual impacting method as the climate chamber should be opened for every measurement.
Applicability of the Method to the Evaluation of Low Temperature Stiffness Modulus of Asphalt Concrete
To assess the repeatability of the measurement at low temperatures, 30 repetitions are performed at 60 s interval on a dummy asphalt concrete specimen of similar geometry. The results indicate high repeatability with standard deviations of 4.7 Hz and 2.4 Hz at − 20 °C and − 30 °C, respectively (Fig. 7). Even though the damping increases with increased measurement temperatures, the repeatability of the resonant frequencies is still satisfactory (4.9 Hz at − 10 °C and 5.1 Hz at 0 °C).
Low temperature measurements on asphalt concrete require a sample to be conditioned at the required temperatures. To set the conditioning time for a single measurement temperature, the resonance of the dummy asphalt specimen was monitored with time. The specimen is positioned in the thermal chamber at room temperature and then the temperature is set to − 20 °C. After waiting for 16 h, a continuously repeated resonant frequency measurement is taken until the values of the results have an average deviation of 0.08%. Then, the temperature is decreased to − 25 °C and repeated measurements are taken until the measured resonant frequency reaches a satisfactorily constant value (Fig. 8). It is to be noted that longer duration is chosen for conditioning the dummy specimen before decreasing the temperature to − 25 °C. This is done in order to obtain a satisfactorily constant reference measurement at − 20 °C.
The above procedure allows the conditioning time to be estimated before the respective measurements are taken on the actual specimen at each temperature. Figure 8 shows the measurements on the dummy sample for the conditioning period. As expected, the resonant frequency of the sample increases with a decrease in temperature due to the increase in the stiffness of the asphalt at lower temperatures. From the result of this measurement, it can be observed that an average deviation of 0.1% (for 5 °C difference) can be achieved within 3 h. Therefore, according to this result, 3 h is considered as an applicable conditioning period.
The measurements on the actual asphalt specimen are taken after the specimen is conditioned for 3 h at each measurement temperature (0 °C to − 40 °C) as per the above finding. With no other form of variation in the measurement, the temperature is decreased by 5 °C from a starting point of 0 °C. It should be noted that the entire test protocol is performed automatically with the temperature chamber kept closed during all measurements at each temperature. The change in resonant frequency is caused only by the reduction in temperature and not by any other modification. This is advantageous, since it is possible to avoid any effects caused by contact between the transducers and the specimen that would disturb the dynamics of the specimen.
It can be observed in Fig. 9 that the decrease in temperature affects the measured resonant frequencies of the specimen. This result shows the expected increase in resonant frequency as the asphalt mixture specimen becomes increasingly stiff with a decrease in temperature. It should be noted in this measurement protocol that the cumulative number of conditioning hours increases while the specimen is kept at these low temperatures. This may cause physical hardening to play a role by increasing the resonant frequencies. However, the temperature effect is considered to be dominant in the results obtained.
Studies on micro-damage associated with low temperature depict the presence of micro-cracks at the aggregate-mastic interfaces as well as within the mastic portion of asphalt concrete after it has been subjected to low temperatures [27]. Hence, it is possible that the measured resonant frequencies can be influenced by the presence of potential micro-damage. However, the main focus of our study is developing the methodology and the topic of micro-damage is out of its scope.
The procedure described in Sect. 2 is used to calculate the complex dynamic moduli of the specimen at each temperature. Poisson’s ratio is assumed to be 0.2 for temperatures below − 20 °C and 0.25 for those above − 20 °C [9]. Figure 10 shows the change in dynamic moduli resulting from an increase in stiffness with a decrease in asphalt temperature. This result shows that the proposed method can be applicable to the study of low temperature effects without any other form of mechanical stress involved.
Figure 11 shows the calculated damping ratios of the measurements according to the half-power bandwidth method (Eq. 3). It can be observed that, with the temperature decreasing, the damping of the measured frequencies becomes less significant. There is a stronger decrease in damping from 0 to − 10 °C, while a smooth and gentle drop is later observed in the measurement temperatures. This shows that the viscous behavior of the specimen is more pronounced above a temperature of − 10 °C. The lower rate of decrease in damping ratio below − 10 °C can be an indication that the specimen becomes more consistently elastic below − 10 °C. The result also indicates the potential use of the proposed testing method to study the viscoelastic behaviors of asphalt concrete with a decrease in temperature.