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Synthesis, Structure, Selective and Sensitive Sensing for Tetracycline of a Zn–MOF

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Abstract

A kind of potential sensor material for tetracycline (TC) in water: {[Zn3(TPA)2(tib)2(HCOO)2]·4(H2O)·0.5(CH2Cl2)}n (Zn-MOF), was successfully constructed under the condition of solvothermal, using 1,3,5-tirs(1-imidazolyl)benzene (tib), and terephthalic acid (H2TPA). Its structure was characterized by X-ray single-crystal diffraction, elemental analysis and IR spectra. The results of analysis showed that Zn-MOF crystallizes in the monoclinic system, C2/c space group and features a 3-nodal (3,3,4)-connected network with point symbol of 2{83}2{86}{8.102}. The fluorescence quenching experimental results showed that Zn-MOF exhibited selective and sensitive response to TC with detection limit of 4.86 × 10− 7 g·L− 1 (equals to 1.09 × 10− 9 M) based on its effective spectral overlap and adsorption preconcentration with tetracycline (TC).

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Acknowledgements

This research was funded by Guangxi Key Laboratory of Urban Water Environment and Guangxi First-class Disciplines (Agricultural Resources and Environment).

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Authors and Affiliations

  1. Guangxi Key Laboratory of Urban Water Environment, College of Chemistry and Environmental Engineering, Baise University, 533000, Baise, China

    Chunhuan Li, Yonggang Li, Kerui Huang, Fang Liu, Yongle Gan & Liansheng Cui

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  1. Chunhuan Li
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  2. Yonggang Li
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  3. Kerui Huang
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  4. Fang Liu
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  5. Yongle Gan
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  6. Liansheng Cui
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Contributions

Chunhuan Li carried out the fluorescence quenching experiments.Yonggang Li wrote the sections “Abstract”, “Keywords” and “Introduction”. Kerui Huang and Fang Liu wrote the section “Experimental” and collating the references.Yongle Gan and Liansheng Cui wrote the section “Results and discussion” and “Conclusion”.All authors reviewed the manuscript.

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Correspondence to Yongle Gan or Liansheng Cui.

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Li, C., Li, Y., Huang, K. et al. Synthesis, Structure, Selective and Sensitive Sensing for Tetracycline of a Zn–MOF. J Inorg Organomet Polym 33, 1586–1591 (2023). https://doi.org/10.1007/s10904-023-02581-4

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