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Assembly of Five Coordination Polymers Based on Furan-2,5-dicarboxylic acid and 4,4′-Azobispyridine: Synthesis, Structures and Luminescence Properties

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Abstract

Five coordination polymers (CPs) {[Zn4(FDA)4(H2O)12]}n (1) {[M(FDA)(azopy)·DMF]}n (2) [M = Zn (2a), Co (2b) and Cd (2c)] and {[Zn(FDA)(azopy)]·CH3CN·0.5DMF}n (3) have been harvested from furan-2,5-dicarboxylic acid (H2FDA) and 4,4′-azobispyridine (azopy), and structurally characterized by infrared spectra, elemental analysis, thermogravimentric analysis, powder X-ray diffraction and single-crystal X-ray diffraction. CP 1 shows an interesting one-dimension chain structure. CP 2a and CP 2b are isostructural and demonstrate two-dimensional 4-connected sql topological structures where FDA2− connected the nearest Zn(II) ions to generate a one-dimension chain and the chains could be further linked by azopy. CP 2c significantly differs from CP 2a and CP 2b in coordination number as well as in the coordination mode of carboxylate groups. However CP 2c can generate the same two-dimensional sql structure as well. While CP 3 is an interesting pillared-layer three-dimensional two-fold interpenetrating framework with a pcu alpha-Po primitive cubic topology. The luminescence properties of CP 1, CP 2a, CP 2c and CP 3 are investigated.

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Acknowledgements

Financial supports from the National Natural Science Foundation of China (Nos. 21561014 and 21562023), the Key Research Project of Jiangxi Province (No. 20171BBF60074) and the Key Research Project of Jiangxi Academy of Sciences (No. 2018-YZD2-11) are greatly acknowledged.

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Authors and Affiliations

  1. Institute of Applied Chemistry, Jiangxi Academy of Sciences, Nanchang, 330096, People’s Republic of China

    Sheng-Yong You, Ling Li, Ji-Yong Zou & Kai-Hong Chen

  2. Key Laboratory of Theoretical Organic Chemistry and Functional Molecule of the Ministry of Education, School of Chemistry and Chemical Engineering, Hunan University of Science and Technology, Xiangtan, 411201, Hunan, People’s Republic of China

    Shao-Wei Zhang

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Appendix A: Supplementary Data

Appendix A: Supplementary Data

CCDC 1843748 for 1, 1843749 for 2a, 1843752 for 2b, 1843750 for 2c, and 1843754 for 3 contain the supplementary crystallographic data of this paper. These data can be obtained free of charge via http://www.ccdc.cam.ac.uk/conts/retrieving.html, or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, UK; fax: (+44) 1223-336-033; or e-mail: deposit@ccdc.cam.ac.uk.

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You, SY., Li, L., Zou, JY. et al. Assembly of Five Coordination Polymers Based on Furan-2,5-dicarboxylic acid and 4,4′-Azobispyridine: Synthesis, Structures and Luminescence Properties. J Inorg Organomet Polym 30, 410–416 (2020). https://doi.org/10.1007/s10904-019-01199-9

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