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Investigation on microwave absorption properties of bismuth ions doped barium hexaferrites

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Abstract

In the present work, we have reported the impact of bismuth (Bi) substitution on the structural, morphological, magnetic and microwave absorption properties of sol–gel route synthesized M-type barium hexaferrite BaBixFe12−xO19 (x = 0.00, 0.05, 0.10 and 0.15) within the frequency range of 1–12.5 GHz. The structure, associated functional groups, surface morphology, elemental composition, magnetic and microwave absorption characteristics, were analysed using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), Field emission scanning electron microscopy (FE-SEM), High resolution transmission electron microscopy (HR-TEM), X-ray Photoelectron Spectroscopy (XPS), Brunauer-Emmett-Teller (BET) analysis, vibrating sample magnetometer (VSM) and vector network analyzer (VNA), respectively. XRD patterns confirmed the single-phase hexagonal structure with high crystallinity and polycrystalline nature of the of bismuth ions doped barium hexaferrites. FE-SEM micrographs indicated that the grains were of platelet-like shapes. The confirmation of particle sizes and shapes were determined by HR-TEM micrographs. XPS investigations elucidated the elemental composition and chemical states at the surface level. BET analysis shed light on the specific surface area and pore characteristics. The increase in saturation magnetization caused by the addition of bismuth dopant is attributed to the replacement of Bi3+ for Fe3+ in tetrahedral 4f1 sites. Microwave absorption characteristics revealed a minimal reflection loss (RL) of nearly − 38.78 dB for a sample thickness of 2.9 mm with an EABRL<− 10 dB of 1.31 GHz (11.46–12.47) and EABRL<− 20 dB of 0.5 GHz (12.05–12.50) near the frequency 12 GHz for x = 0.10 displaying the highest reflection loss of all compositions. The minimum RL lower than − 10 dB and − 20 dB shows that more than 90% and 99% of the electromagnetic wave energy is absorbed. Therefore, this investigation sheds light on the multifaceted influence of bismuth doping on the structural, morphological, magnetic and microwave absorption properties of M-type barium hexaferrites, offering significant implications for their utilization in various technological applications, particularly in the realm of microwave absorption.

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Data availability

On reasonable request, the corresponding author will make available the data sets created and/or analysed during the current work.

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Acknowledgements

Mr. Rohit, one of the authors, is grateful to the University Grant Commission, Government of India, for giving financial support in the form of a Junior Research Fellowship under Reference No. 4837/(CSIR-UGC NET DEC. 2018).

Funding

Funding was provided by University Grants Commission—South Eastern Regional Office, 4837/(CSIR-UGC NET DEC. 2018).

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Authors and Affiliations

  1. Department of Physics, Himachal Pradesh University, Shimla, 171005, India

    Rohit Duglet, Deepika Sharma, Anjali Thakur & M. Singh

  2. Faculty of Allied Health Sciences, Chettinad Hospital and Research Institute, Chettinad Academy of Research and Education, Kelambakkam, Tamilnadu, 603103, India

    Ankush Chauhan

  3. Centre for Herbal Pharmacology and Environmental Sustainability, Chettinad Hospital and Research Institute, Chettinad Academy of Research and Education, Kelambakkam, Tamilnadu, 603103, India

    Ankush Chauhan

Authors
  1. Rohit Duglet
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  2. Ankush Chauhan
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  4. Anjali Thakur
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  5. M. Singh
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Contributions

Conceptualization and design of research article were contributed by all authors. Synthesis of samples were performed by RD and AC. XRD and morphology investigations were performed by RD, DS and AT. Elements compositional variation and surface area analyses were performed by RD. Magnetic investigations were performed by AC and RD. Microwave absorption investigations were performed by RD, DS and AT. Writing, editing and original draft were prepared by RD, AC and MS. The final version of the manuscript has been read, agreed upon, and approved by all authors.

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Correspondence to Rohit Duglet or M. Singh.

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Duglet, R., Chauhan, A., Sharma, D. et al. Investigation on microwave absorption properties of bismuth ions doped barium hexaferrites. J Mater Sci: Mater Electron 35, 654 (2024). https://doi.org/10.1007/s10854-024-12418-6

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