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Influence of heat treatment temperatures on microstructure and characterization of BaFe2 2+Fe15.6 3+O26.4 hexaferrite

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Abstract

A series of W-type hexagonal ferrites with composition BaFe2 2+Fe15.6 3+O26.4 at different temperatures was synthesized via a ceramic process in a reducing atmosphere during the whole process of calcination and sintering. The phase identification of magnetic powders was performed by X-ray diffraction. The result of XRD confirmed the appearance of a pure phase hexagonal crystal structure with temperature from 1290 to 1330 °C. The microstructures of the magnets were investigated by using a HS-4800 scanning electron microscopy. The magnetic properties of the magnets were measured by a permanent magnetic measurement equipment. B–H curves show that the magnetic properties such as remanence, magnetic induction coercivity, intrinsic coercivity, saturation magnetization and maximum energy product are significantly affected by calcination and sintering temperatures. The optimized sintering and calcination temperatures are 1280 and 1300 °C, respectively.

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References

  1. P.W. Anderson, Phys. Rev. 102, 1008–1013 (1956)

    Article  Google Scholar 

  2. X. Liu, W. Zhong, B. Gu, Y. Du, J. Appl. Phys. 92, 1028–1032 (2002)

    Article  Google Scholar 

  3. M. Pardavi-Horvath, J. Magn. Magn. Mater. 171, 215–216 (2000)

    Google Scholar 

  4. R.C. Pullar, Prog. Mater. Sci. 57, 1191–1334 (2012)

    Article  Google Scholar 

  5. X.S. Liu, P. Hernández-Gómez, K. Huang, S. Zhou, Y. Wang, X. Cai, H. Sun, B. Ma, J. Magn. Magn. Mater. 305, 524–528 (2006)

    Article  Google Scholar 

  6. F. Lv, X. Liu, S. Feng, Mater. Lett. 157, 277–280 (2015)

    Article  Google Scholar 

  7. D.M. Hemeda, A. Al-Sharif, O.M. Hemeda, J. Magn. Magn. Mater. 315, 1–7 (2007)

    Article  Google Scholar 

  8. L.A. Bashkirov, G.P. Dudchik, T.A. But’ko, L.Y. Kris’ko et al., Inorg. Mater. 39, 525–528 (2003)

    Article  Google Scholar 

  9. D. Lisjak, A. Žnidaršič, A. Sztanislav, M. Drofenik, J. Eur. Ceram. Soc. 28, 2057–2062 (2008)

    Article  Google Scholar 

  10. P.B. Braun, Philos Res. Rep. 12, 491(1957)

    Google Scholar 

  11. F.K. Lotgering, P.H.G.M. Vromans, M.A.H. Huyberts, J. Appl. Phys. 51, 5913–5918 (1980)

    Article  Google Scholar 

  12. G. Albanese, M. Carbucicchio, G. Asti, Appl. Phys. 11, 81–88 (1976)

    Article  Google Scholar 

  13. S. Ram, J.C. Joubert, J. Magn. Magn. Mater. 99, 133–144 (1991)

    Article  Google Scholar 

  14. T.T.V. Nga, N.P. Duong, T.D. Hien, J. Alloys Compd. 475, 55–59 (2009)

    Article  Google Scholar 

  15. P. Sharma, A. Verma, R.K. Sidhu, O.P. Pandey, J. Magn. Magn. Mater. 307, 157–164 (2006)

    Article  Google Scholar 

  16. Z.F. Zi, Y.P. Sun, X.B. Zhu, Z.R. Yang, J.M. Dai, W.H. Song, J. Magn. Magn. Mater. 320, 2746–2751(2008)

    Article  Google Scholar 

  17. K. Haneda, H. Kojima, J. Appl. Phys. 44, 3760–3762 (1973)

    Article  Google Scholar 

  18. X. Niu, X. Liu, S. Feng, Optik 126, 5513–5516(2015)

    Article  Google Scholar 

  19. Y. Yang, X. Liu, D. Jin, J. Magn. Magn. Mater. 364, 11–17 (2014)

    Article  Google Scholar 

  20. Y.W. Du, Ferrite (Jiangsu Science and Technology Press, Nanjing, 1995)

    Google Scholar 

  21. A.P. Lilot, A. Gérard, F. Grandjean, IEEE Trans. Magn. 18, 1463–1465 (1982)

    Article  Google Scholar 

  22. V.N. Dhage, M.L. Mane, A.P. Keche, C.T. Birajdar, K.M. Jadhav Phys. B 406, 789–793 (2011)

    Article  Google Scholar 

  23. S. Kumar, T. Kaur, S. Kumar, A.K. Srivastava. J. Supercond. Nov. Magn. 28, 2935–2940 (2015)

    Article  Google Scholar 

  24. M.R. Meshram, N.K. Agrawal, B. Sinha, P.S. Misra, J. Magn. Magn. Mater. 271, 207–214 (2004)

    Article  Google Scholar 

  25. M.J. Iqbal, S. Farooq, Mater. Res. Bull. 46, 662–667 (2011)

    Article  Google Scholar 

  26. A. Haq, M. Anis-ur-Rehman, Phys. B 407, 822–826 (2012)

    Article  Google Scholar 

Download references

Acknowledgements

This work was supported by the National Natural Science Foundation of China (Nos. 51472004, 51272003).

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Authors and Affiliations

  1. Engineering Technology Research Center of Magnetic Materials, School of Physics & Materials Science, Anhui University, Hefei, 230601, Anhui, People’s Republic of China

    Jin Tang, Xiansong Liu, Khalid Mehmood Ur Rehman, Mingling Li, Cong Zhang, Xiangyu Meng, Haohao Li & Chaocheng Liu

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  1. Jin Tang
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  2. Xiansong Liu
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  3. Khalid Mehmood Ur Rehman
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  4. Mingling Li
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  5. Cong Zhang
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  8. Chaocheng Liu
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Correspondence to Xiansong Liu.

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Tang, J., Liu, X., Rehman, K.M.U. et al. Influence of heat treatment temperatures on microstructure and characterization of BaFe2 2+Fe15.6 3+O26.4 hexaferrite. J Mater Sci: Mater Electron 28, 12086–12091 (2017). https://doi.org/10.1007/s10854-017-7021-4

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