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Simple new synthesis of nickel oxide (NiO) in water using microwave irradiation

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Abstract

NiO with spherical-like morphology were prepared by microwave irradiation using Ni(II) acetate, water as solvent and sodium hydroxide (NaOH) as precipitator agent. Structural, optical and nanostructures were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), UV–Vis absorption; Fourier transformed infrared (FTIR). The XRD pattern studies revealed the NiO have a face-centered cubic structure. The composition of nanostructures confirmed by analysis of FTIR spectra. The average size of the NiO nanoparticle observed from SEM images is found to be dimensions about 20 nm.

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Authors and Affiliations

  1. School of Physics, Damghan University, Damghan, 36716-41167, Iran

    Soheil Allahyar & Amir Abharya

  2. Departments of Chemistry, Islamic Azad University, Yazd Branch, Yazd, 89195-155, Iran

    Milad Taheri

  3. Departments of Chemistry, Islamic Azad University, Gorgan Branch, Gorgan, 49147-39975, Iran

    Kolsom Mohammadi

Authors
  1. Soheil Allahyar
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  2. Milad Taheri
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  3. Amir Abharya
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  4. Kolsom Mohammadi
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Correspondence to Soheil Allahyar.

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Allahyar, S., Taheri, M., Abharya, A. et al. Simple new synthesis of nickel oxide (NiO) in water using microwave irradiation. J Mater Sci: Mater Electron 28, 2846–2851 (2017). https://doi.org/10.1007/s10854-016-5868-4

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  • DOI: https://doi.org/10.1007/s10854-016-5868-4

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