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Detection of Zinc in Food Based on High-Stability Zinc Coordination Supramolecular Self-Assembled Polymerenhanced Resonance Light Scattering

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Journal of Applied Spectroscopy Aims and scope

The resonance light scattering method was used to study the coordination-driven self-assembly reaction of zinc with a bipolar tetradentate ligand and a bipolar bidentate ligand to form a supramolecular polymer. The bipolar tetradentate ligand was N,N’-bis(pyridoxal phosphate)-o-tetraminobiphenyl synthesized by the reaction of pyridoxal phosphate with biphenyltetramine, and the bipolar bidentate ligand was bis-phenanthroline-glutaraldehyde synthesized by the reaction of glutaraldehyde with 5-aminophe-nanthroline. The formation of the supramolecular polymer causes signal enhancement of resonance light scattering. Based on this, we established a new method for the determination of zinc by resonance light scattering. Under optimized experimental conditions, the zinc concentration in the range of 0.3–30 ng/mL showed a good linear relationship with the resonance light scattering intensity of the system. The detection limit of the method is 0.1 ng/mL. Using this method to determine the content of zinc in food, the recovery rate of standard addition is between 95 and 107%, and the relative standard deviation is less than 3.68%.

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Authors and Affiliations

  1. Hengyang Market Supervision, Inspection and Testing Center, Hengyang, China

    Jing Yang & Lizhen Nie

  2. School of Chemistry and Chemical Engineering at University of South China, Hengyang, China

    Qian Li, Canhui Xu, Chen Liu, Changming Nie, Xin Zhou & Lifu Liao

  3. School of Resource & Environment and Safety Engineering at University of South China, Hengyang, China

    Yujie Li

  4. Hunan Key Laboratory of Typical Environmental Pollution and Health Hazards, School of Public Health, Hengyang Medical School, University of South China, Hengyang, Hunan Province, China

    Xilin Xiao

Authors
  1. Jing Yang
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  2. Qian Li
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  3. Canhui Xu
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  4. Yujie Li
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  5. Lizhen Nie
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  6. Chen Liu
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  7. Xilin Xiao
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  8. Changming Nie
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  9. Xin Zhou
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  10. Lifu Liao
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Corresponding authors

Correspondence to Xilin Xiao or Lifu Liao.

Additional information

Abstract of article is published in Zhurnal Prikladnoi Spektroskopii, Vol. 89, No. 6, p. 906, November–December, 2022.

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Yang, J., Li, Q., Xu, C. et al. Detection of Zinc in Food Based on High-Stability Zinc Coordination Supramolecular Self-Assembled Polymerenhanced Resonance Light Scattering. J Appl Spectrosc 89, 1232–1240 (2023). https://doi.org/10.1007/s10812-023-01490-1

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  • DOI: https://doi.org/10.1007/s10812-023-01490-1

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