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Direct determination of lead in wine materials by atomic absorption spectrometry using an electrothermal atomizer with a graphite filter-insert

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Journal of Applied Spectroscopy Aims and scope

The operational parameters of an atomizer with a graphite filter-insert and a Pd-Mg matrix modifier are optimized for direct electrothermal atomic absorption determination of lead in some wines and associated materials. A method is proposed for eliminating interferences from mineral and organic components, as well as from nonatomic absorption, and for increasing the detection sensitivity for the element by up to a factor of two. The lower limit for determining the amount of lead in wines is 0.0025 mg/dm3. The relative standard deviation (S r) does not exceed 10%.

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Authors and Affiliations

  1. I. I. Mechnikov Odessa National University, 2 Dvoryanskaya Str., Odessa, 65026, Ukraine

    A. N. Zacharia, A. S. Zhuravlev, A. N. Chebotarev & M. V. Arabadgi

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  1. A. N. Zacharia
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  2. A. S. Zhuravlev
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  3. A. N. Chebotarev
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  4. M. V. Arabadgi
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Correspondence to A. N. Zacharia.

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Translated from Zhurnal Prikladnoi Spektroskopii, Vol. 79, No. 6, pp. 953–958, November–December, 2012.

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Zacharia, A.N., Zhuravlev, A.S., Chebotarev, A.N. et al. Direct determination of lead in wine materials by atomic absorption spectrometry using an electrothermal atomizer with a graphite filter-insert. J Appl Spectrosc 79, 949–954 (2013). https://doi.org/10.1007/s10812-013-9708-5

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  • DOI: https://doi.org/10.1007/s10812-013-9708-5

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