The structure of a new compound was determined using PMR and 13C NMR spectroscopy (HHCOSY, HSBC, HMBC, ROESY) as 2-[3′-methoxy,4-O-β-D-galactopyranos-1-yl)benzyl]-3-(3″,4″-dimethoxybenzyl)-4hydroxybutyric acid, which was isolated for the first time from seeds of Scotch thistle Onopordum acanthium L.
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Acknowledgment
We thank A. Z. Khalilova and A. A. Muldashev for help in collecting and identifying the plant material and Doctor of Chemical Sciences Prof. A. S. Shashkov for supplying the 2D NMR results.
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*For No. XII, see [1].
Translated from Khimiya Prirodnykh Soedinenii, No. 1, pp. 53–55, January–February, 2009.
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Tyumkina, T.V., Nuriev, I.F., Khalilov, L.M. et al. PMR and 13C NMR spectra of biologically active compounds. XIII.* Structure and stereochemistry of a new phenylpropanoid glycoside isolated from Onopordum acanthium seeds. Chem Nat Compd 45, 61–65 (2009). https://doi.org/10.1007/s10600-009-9254-9
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DOI: https://doi.org/10.1007/s10600-009-9254-9