The stability of steady thermal conditions of 2-ethylhexanol nitration in a laboratory unit with a centrifugal mass-transfer device was analyzed. It was found that the chemical reaction is stable during nitration of the alcohol in the 273–293 K temperature range. In the 285–295 K temperature range, the target product (2-ethylhexyl nitrate) yield reaches 92% with 99.4% purity.
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Translated from Khimicheskoe i Neftegazovoe Mashinostroenie, Vol. 58, No. 3, pp. 3–5, March, 2022.
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Karpov, A.G., Vasilishin, M.S., Ivanov, O.S. et al. Assessment of Stability of Thermal Conditions of 2-Ethylhexanol Nitration. Chem Petrol Eng 58, 175–178 (2022). https://doi.org/10.1007/s10556-022-01072-6
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DOI: https://doi.org/10.1007/s10556-022-01072-6