Table 3 Experimental matrix and the resulting La, Ce, Nd, Y, and TREE leaching efficiencies (%)
Te st number | C (%) | T (°C ) | t (mins) | S/L ratio (g mL−1) | La (%) | Ce (%) | Nd (%) | Y (%) | TREE (%) |
|---|---|---|---|---|---|---|---|---|---|
1 | 1 | 28 | 120 | 1:5 | 16.5 ± 1.1 | 11.9 ± 1.2 | 12.9 ± 1.4 | 13.7 ± 0.6 | 13.7 ± 0.9 |
2 | 2.5 | 28 | 120 | 1:5 | 30.8 ± 0.7 | 26.1 ± 0.9 | 26.5 ± 0.8 | 30.4 ± 0.8 | 28.4 ± 0.6 |
3 | 5 | 28 | 120 | 1:5 | 39.7 ± 2.1 | 35.8 ± 2.3 | 35.2 ± 2.0 | 40.3 ± 1.6 | 37.7 ± 1.9 |
4 | 10 | 28 | 120 | 1:5 | 58.7 ± 4.8 | 57.6 ± 5.0 | 52.7 ± 4.2 | 56.4 ± 3.7 | 55.9 ± 4.3 |
5 | 10 | 40 | 120 | 1:5 | 62.4 ± 0.7 | 61.3 ± 0.8 | 55.9 ± 0.8 | 58.5 ± 0.8 | 58.8 ± 0.8 |
6 | 10 | 50 | 120 | 1:5 | 74.6 ± 2.9 | 72.4 ± 2.5 | 70.6 ± 3.6 | 68.2 ± 2.5 | 71.0 ± 2.9 |
7 | 10 | 60 | 120 | 1:5 | 69.5 ± 5.5 | 67.6 ± 4.8 | 64.4 ± 7.1 | 63.2 ± 4.2 | 65.6 ± 5.5 |
8 | 10 | 70 | 120 | 1:5 | 64.8 ± 2.7 | 63.6 ± 2.3 | 58.4 ± 3.6 | 59.0 ± 1.9 | 60.8 ± 2.6 |
9 | 10 | 80 | 120 | 1:5 | 73.3 ± 5.9 | 70.9 ± 5.5 | 68.9 ± 7.0 | 66.1 ± 5.3 | 69.2 ± 6.0 |
10 | 10 | 50 | 5 | 1:5 | 57.7 ± 2.1 | 53.8 ± 2.3 | 49.5 ± 2.2 | 52.4 ± 1.4 | 52.9 ± 1.9 |
11 | 10 | 50 | 15 | 1:5 | 62.6 ± 0.2 | 58.7 ± 0.2 | 53.6 ± 1.0 | 56.2 ± 0.8 | 57.1 ± 0.5 |
12 | 10 | 50 | 30 | 1:5 | 63.0 ± 0.2 | 59.2 ± 0.5 | 53.9 ± 0.3 | 57.1 ± 0.8 | 57.6 ± 0.5 |
13 | 10 | 50 | 45 | 1:5 | 64.1 ± 0.3 | 60.4 ± 0.1 | 55.4 ± 0.3 | 58.5 ± 0.7 | 59.0 ± 0.3 |
14 | 10 | 50 | 60 | 1:5 | 63.9 ± 0.9 | 60.4 ± 0.7 | 55.3 ± 1.3 | 57.6 ± 0.8 | 58.7 ± 0.8 |
15 | 10 | 50 | 30 | 1:2 | 61.4 ± 0.8 | 59.4 ± 0.8 | 52.5 ± 0.9 | 57.5 ± 0.5 | 57.2 ± 0.7 |
16 | 10 | 50 | 30 | 1:3 | 63.9 ± 0.8 | 61.7 ± 0.9 | 55.1 ± 0.6 | 59.9 ± 1.1 | 59.6 ± 0.8 |
17 | 10 | 50 | 30 | 1:4 | 64.0 ± 0.2 | 62.0 ± 0.2 | 55.5 ± 0.3 | 59.8 ± 0.6 | 59.7 ± 0.1 |
18 | 10 | 50 | 30 | 1:10 | 65.5 ± 0.5 | 63.4 ± 0.4 | 57.0 ± 0.4 | 60.8 ± 0.7 | 61.1 ± 0.5 |