Skip to main content
SpringerLink
Log in

Easy and low-cost preparation method of magnetic montmorillonite/FexOy composite: initial study for future applications

  • Original Paper
  • Published:
Monatshefte für Chemie - Chemical Monthly Aims and scope Submit manuscript

Abstract

Magnetic montmorillonite with FexOy nanoparticles was prepared by precipitation. The results of the leaching test showed that the magnetic montmorillonite is stable in the acidic pH. The microwave treatment and the presence of FexOy nanoparticles on the montmorillonite did not influence the montmorillonite structure or distinctive release of the monitored cations. The main goal of the present paper was to find the optimal solid-to-liquid ratio when the ionic strength remains unchanged. The influence of solid-to-liquid ratio, leaching time, initial pH of extraction agent and the variation of the ionic strength of the final extract were studied as well. The results evaluated by analysis of variance (ANOVA) showed that both the solid-to-liquid ratio and the initial pH are factors which significantly influence the release of the cations from the study materials as well as the ionic strength of final extracts.

Graphic abstract

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9

Similar content being viewed by others

References

  1. Lin S-H, Juang R-S (2002) J Hazard Mater 92:315

    Article  CAS  Google Scholar 

  2. Oliveira LCA, Rios RVRA, Fabris JD, Sapag K, Garg VK, Lago RM (2003) Appl Clay Sci 22:169

    Article  CAS  Google Scholar 

  3. Ijagbemi CHO, Baek M-H, Kim D-S (2009) J Hazard Mater 166:538

    Article  CAS  Google Scholar 

  4. Bhattacharya AK, Mandal SN, Das SK (2006) Chem Eng J 123:43

    Article  CAS  Google Scholar 

  5. Kalantari K, Ahmad MB, Masoumi HRF, Shameli K, Basri M, Khandanlou R (2015) Chem Eng 49:192

    CAS  Google Scholar 

  6. Sizmur T, Fresno T, Akgül G, Frost H, Moreno-Jiménez E (2017) Bioresour Technol 246:34

    Article  CAS  Google Scholar 

  7. Seidlerová J, Šafařík I, Rozumová L, Šafaříková M, Motyka O (2016) Procedia Mater Sci 12:147

    Article  Google Scholar 

  8. Lee SM, Laldawngliana C, Tiwari D (2012) Chem Eng J 195–196:103

    Article  Google Scholar 

  9. Mockovčiaková A, Orolínová Z, Škvarla J (2010) J Hazard Mater 180:274

    Article  Google Scholar 

  10. Pirillo S, Cornaglia L, Ferreira ML, Rueda EH (2008) Spectrochim Acta Part A 71:636

    Article  Google Scholar 

  11. Momtazi L, Bagherifam S, Singh G, Hofgaard A, Hakkarainen M, Glomm WR, Ross N, Mælandsmo GM, Griffiths G, Nyström B (2014) J Colloid Interface Sci 433:76

    Article  CAS  Google Scholar 

  12. Singh KK, Senapati KK, Sarma KC (2017) J Environ Chem Eng 5:2214

    Article  CAS  Google Scholar 

  13. Luther S, Borgfeld N, Kim J, Parsons JG (2012) Microchem J 101:30

    Article  CAS  Google Scholar 

  14. Safarik I, Horska K, Pospiskova K, Safarikova M (2012) Powder Technol 229:285

    Article  CAS  Google Scholar 

  15. Bourlinos AB, Karakassides MA, Simopoulos A, Petridis D (2000) Chem Mater 12:2640

    Article  CAS  Google Scholar 

  16. Gao Z, Li X, Wu H, Zhao S, Asuha S (2015) Microporous Mesoporous Mater 202:1

    Article  CAS  Google Scholar 

  17. Rahimi Z, Sarafraz H, Sarafraz Gh, Shirani AS (2018) J Radioanal Nucl Chem 44:722

    Google Scholar 

  18. Majidi S, Sehrig FZ, Farkhani SM, Goloujeh MS, Akbarzadeh A (2016) Artif Cells Nanomed Biotechnol 44:722

    Article  CAS  Google Scholar 

  19. Yu M, Wang L, Hu L, Li Y, Luo D, Mei S (2019) Trends Anal Chem 119:115611

    Article  CAS  Google Scholar 

  20. Safarik I, Safarikova M (2014) Int J Mat Res 105:104

    Article  CAS  Google Scholar 

  21. Tokarčíková M, Tokarský J, Kutláková KM, Seidlerová J (2017) J Solid State Chem 253:329

    Article  Google Scholar 

  22. Klika Z, Seidlerová J, Valášková M, Kliková CH, Kolomazník I (2016) Appl Clay Sci 132–133:41

    Article  Google Scholar 

  23. Tokarčíková M, Tokarský J, Čabanová K, Matějka V, Mamulová Kutláková K, Seidlerová J (2014) Compos B 67:262

    Article  Google Scholar 

  24. White AF, Peterson ML, Hochella MF (1994) Geochim Cosmochim Acta 58:1859

    Article  CAS  Google Scholar 

  25. Prince AAM, Velmurugan S, Narasimhan SV, Ramesh C, Murugesan N, Raghavan PS, Gopalan R (2001) J Nucl Mater 289:281

    Article  CAS  Google Scholar 

  26. Zhou Q, Wang Y, Bierwagen GP (2012) Corros Sci 55:97

    Article  CAS  Google Scholar 

  27. Hasson D, Bendrihem O (2006) Desalination 190:189

    Article  CAS  Google Scholar 

  28. Withers A (2005) Desalination 179:11

    Article  CAS  Google Scholar 

  29. Pospiskova K, Safarik I (2015) Mater Lett 142:184

    Article  CAS  Google Scholar 

  30. Valášková M, Hundáková M, Mamulová MK, Seidlerová J, Čapková P, Pazdziora E, Matějová K, Heřmánek M, Klemm V, Rafaja D (2010) Geochim Cosmochim Acta 10:6287

    Article  Google Scholar 

  31. Czech Office for Standards, Metrology and Testing (1992) SOP č.OAA-02-13. Nanotechnology Centre, VSB-TU, Ostrava

  32. R Core Team (2018) R: a language and environment for statistical computing. R Foundation for Statistical Computing, Vienna, Austria. https://www.R-project.org/

Download references

Acknowledgements

The work was supported by ERDF/ESF New Composite Materials for Environmental Applications (No. CZ.02.1.01/0.0/0.0/17_048/0007399).

Author information

Authors and Affiliations

  1. Nanotechnology Centre, VŠB-Technical University of Ostrava, 17. listopadu 15/2172, 708 00, Ostrava-Poruba, Czech Republic

    Michaela Tokarčíková, Jana Seidlerová, Oldřich Motyka, Klára Drobíková & Kateřina Mamulová Kutláková

  2. Department of Physics, VŠB-Technical University of Ostrava, 17. listopadu 15/2172, 708 00, Ostrava-Poruba, Czech Republic

    Ondřej Životský

Authors
  1. Michaela Tokarčíková
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Jana Seidlerová
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Oldřich Motyka
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Ondřej Životský
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. Klára Drobíková
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. Kateřina Mamulová Kutláková
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Michaela Tokarčíková.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Electronic supplementary material

Below is the link to the electronic supplementary material.

Supplementary file1 (DOCX 28 kb)

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Tokarčíková, M., Seidlerová, J., Motyka, O. et al. Easy and low-cost preparation method of magnetic montmorillonite/FexOy composite: initial study for future applications. Monatsh Chem 151, 1–10 (2020). https://doi.org/10.1007/s00706-019-02536-x

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s00706-019-02536-x

Keywords

Search

Navigation