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Magnetically recoverable nano-sized mesoporous solid acid: effective catalysts for the synthesis of 1-amidoalkyl-2-naphthols

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Abstract

Magnetic mesoporous solid acid, SO3H-MCM-41@NiFe2O4, was prepared and characterized by transmission electron microscopy, X-ray diffraction, N2 adsorption–desorption, and hysteresis loop. Under optimized reaction conditions, three-component condensation of aromatic aldehydes with 2-naphthol and benzamides gave corresponding 1-amidoalkyl-2-naphthols in satisfactory to excellent yields. Catalyst could be recovered by magnetic separation and reused for new runs without significant decrease in activity.

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Acknowledgments

Financial support for this work from National Basic Research Program of China (973 Program) (Grant 2010CB126101) is gratefully acknowledged.

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Authors and Affiliations

  1. Shanghai Key Laboratory of Chemical Biology, School of Pharmacy, East China University of Science and Technology, Shanghai, 200237, People’s Republic of China

    Zhixiang Cai, Chen Shu & Yanqing Peng

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  1. Zhixiang Cai
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  2. Chen Shu
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  3. Yanqing Peng
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Corresponding author

Correspondence to Yanqing Peng.

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Cai, Z., Shu, C. & Peng, Y. Magnetically recoverable nano-sized mesoporous solid acid: effective catalysts for the synthesis of 1-amidoalkyl-2-naphthols. Monatsh Chem 145, 1681–1687 (2014). https://doi.org/10.1007/s00706-014-1246-1

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  • DOI: https://doi.org/10.1007/s00706-014-1246-1

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