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Thionation of tetrakis[(ethoxycarbonyl)methoxy]tetrathiacalix[4]arenes with Lawesson’s reagent

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Abstract

Tetra- and tri-thioated derivatives of tetrakis[(ethoxycarbonyl)methoxy]tetrathiacalix[4]arenes were synthesized by thionation with Lawesson’s reagent in dry toluene. The prepared compounds’ structures were investigated by FT-IR, 1H NMR, 2D-NMR, MALDI-TOF-MS, and X-ray crystallography.

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Authors and Affiliations

  1. Chemistry Department, Faculty of Science, Sohag University, Sohag, Egypt

    Omran A. Omran

  2. Chemistry and Environmental Engineering, Department of Biotechnology, Aalborg University, Aalborg, Denmark

    Kim L. Larsen, Reinhard Wimmer & Donghong Yu

Authors
  1. Omran A. Omran
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  2. Kim L. Larsen
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  3. Reinhard Wimmer
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  4. Donghong Yu
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Corresponding author

Correspondence to Omran A. Omran.

Additional information

Correspondence: Omran A. Omran, Chemistry Department, Faculty of Science, Sohag University, Sohag 82524 Egypt.

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Omran, O., Larsen, K., Wimmer, R. et al. Thionation of tetrakis[(ethoxycarbonyl)methoxy]tetrathiacalix[4]arenes with Lawesson’s reagent. Monatsh Chem 139, 1103–1108 (2008). https://doi.org/10.1007/s00706-008-0901-9

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  • DOI: https://doi.org/10.1007/s00706-008-0901-9

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