Abstract
Epitaxial (epi) stacking faults on silicon wafers with <100>- and <111>-orientation were induced by intentional contamination with substances relevant for wafer manufacturing. The resulting defects were investigated by combining optical microscopy, atomic force microscopy and scanning electron microscope Auger electron spectroscopy. The latter was used to investigate the stacking faults both at the outside and in the interior by sputtering with argon ions. The results demonstrate that the type of an epi defect depends on the chemical composition and the physical phase of the contamination.
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Herman MA, Richter W, Sitter H (2004) Epitaxy, physical principles and technical implementation. Springer-Verlag, Berlin Heidelberg New York
Siffert P, Krimmel E (2004) Silicon, evolution and future of a technology. Springer-Verlag, Berlin Heidelberg New York
Chang CY, Sze SM (1996) ULSI technology. McGraw-Hill, New York
Gräf D, Lambert U, Brohl M, Ehlert A, Wahlich R, Wagner P (1996) Comparison of high temperature annealed Czochralski silicon wafers and epitaxial wafers. Mater Sci Eng B 36:50–54
Seacrist M (2005) Silicon starting materials for sub-65 nm technology nodes. Proceedings of the SCP Symposium
Ryuta J, Morita E, Tanaka T, Shimanuki Y (1990) Crystal-originated singularities on Si wafer surface after SC1 cleaning. Jpn J Appl Phys 29:L1947–L1949
Iwabuchi M, Mizushima K, Mizuno M, Kitagawara Y (2000) Dependence of epitaxial layer defect morphology on substrate particle contamination of Si epitaxial wafer. J Electrochem Soc 147:1199–1203
Kimura M, Shinyashiki H, Shimanuki Y (1997) Behavior of COP pits during Si epitaxial growth. Journal of the Japanese Association of Crystal Growth 24:444–448
Imai M, Inoue K, Mayusumi M, Gima S, Nakahara S (2000) Surface imperfection behavior during the SiH4 epitaxial growth process. J Electrochem Soc 147:1568–1572
Sato S, Mizushima I, Miyano K, Sato T, Nakamura S, Tsunashima Y, Arikado T, Uchitomi N (2005) Defects induced by carbon contamination in low-temperature epitaxial silicon films grown with monosilane. Jpn J Appl Phys 44:1169–1173
Murota J (2001) Epitaxial growth techniques: low-temperature epitaxy. In: Crippa D, Rode DL, Masi M (eds) Silicon epitaxy, semiconductors and semimetals. Academic, San Diego, pp 127–149
Glasper JL, Robbins DJ, Pidduck AJ (1992) Calcium contamination of silicon epitaxy. Semicond Sci Technol 7:452–459
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Patsch, B., Ehlert, A., Kirchner, R. et al. Microscale investigation of surface contaminations during silicon epitaxial growth. Microchim Acta 164, 439–444 (2009). https://doi.org/10.1007/s00604-008-0080-8
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DOI: https://doi.org/10.1007/s00604-008-0080-8