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Development and characterization of thin film composite developed from poly (vinyl alcohol) (PVA)/polyethylene glycol (PEG)/norbixin (NBx)/hydroxyapatite

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Abstract

The advancement of the technology of biomaterials has significantly increased, which allows the development of materials that can be used to repair body parts, increase treatments, and improve the quality of human’s life. This study aimed to characterize poly (vinyl alcohol) (PVA) thin films unprecedented added with polyethylene glycol (PEG), norbixin (NBx) and Hydroxyapatite (HA). The systems were prepared by the casting technique and later characterized by FTIR, DRX, thermogravimetry (TG), differential scanning calorimetry (DSC), and optical microscopy (MO). The FTIR results demonstrated that the blends showed satisfactory band displacements with PEG insertion, as well as the peak intensity in relation to the PVA matrix. By XRD, it was possible to observe a displacement to larger angles with the insertion of PEG in relation to the PVA. The films showed a smooth and homogeneous surface. The structures have shown that they may be a desirable option for bone tissue restoration and reconstruction.

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Acknowledgment

The authors wish to express their gratitude to the institutions, IFPI, UFPI, and UEMA for the collaboration and support for this research work.

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Authors and Affiliations

  1. Instituto Federal do Piaui (IFPI)/ Campus Teresina Central, PI, 64001-270, Teresina, Brazil

    Raimundo Miguel da Silva Júnior

  2. Programa de Pós-Graduação em Engenharia de Materiais, Universidade Federal do Piauí (UFPI)/Campus Universitário Ministro Petrônio Portella, Teresina, PI, 64.049-550, Brazil

    Raimundo Miguel da Silva Júnior, Igor Frederico da Silveira Ramos & Gustavo Fernandes de Sousa

  3. Universidade Estadual do Maranhão (UEMA)/Campus Caxias, Caxias, MA, 65.604-380, Brazil

    Deuzuita dos Santos Freitas Viana

  4. Faculdade Integral Diferencia (Facid)/R. Veterinário Bugyja Brito, 1354, - Horto, Teresina, PI, 64052-410, Brazil

    Deuzuita dos Santos Freitas Viana

  5. Programa de Pós-Graduação em Engenharia de Materiais, Instituto Federal do Piaui (IFPI)/ Campus Teresina Central, PI, 64001-270, Teresina, Brazil

    Deuzuita dos Santos Freitas Viana, Ana Larisse Nunes dos Santos, Janiel Costa da Silva & Vicente Galber Freitas Viana

  6. Programa de Pós-Graduação em Engenharia de Materiais, Universidade Federal do Piauí (UFPI)/Campus Ministro Reis Velloso, Av. São Sebastião, n° 2819 - Nossa Sra. de Fátima, Parnaíba, PI, 64202-020, Brazil

    Durcilene Alves da Silva

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  1. Raimundo Miguel da Silva Júnior
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da Silva Júnior, R.M., dos Santos Freitas Viana, D., da Silva, D.A. et al. Development and characterization of thin film composite developed from poly (vinyl alcohol) (PVA)/polyethylene glycol (PEG)/norbixin (NBx)/hydroxyapatite. Colloid Polym Sci 299, 751–762 (2021). https://doi.org/10.1007/s00396-020-04777-3

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