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Preparation, performance and structure-properties relationship of polyphenylene sulfide/ATP-PS/co-deposition of tannic acid nanocomposites membrane

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Abstract

Modified attapulgite (ATP-PS) grafted with polystyrene (PS) was prepared based on Pickering emulsion polymerization. The characterization of ATP-PS was studied by transmission electronic microscopy (TEM), X-ray photoelectron spectrometer (XPS), Fourier transform infrared spectrometer (FTIR) and contact angle analysis. TEM analysis showed that the surface of ATP-PS was coated with PS organic layer; XPS analysis showed that the proportion of C element in ATP-PS was much larger than that of ATP; FTIR analysis found that ATP-PS had more PS specific functional group peaks than that of ATP; Moreover, contact angle results showed that the hydrophobicity of ATP-PS was significantly improved compared with ATP. The above characterization analysis proved that the modification of ATP-PS was successful. Moreover, polyphenylene sulfide (PPS) hydrophobic porous membrane was prepared with 1-chloronaphthalene and dibutyl phthalate as mixed diluents and ATP-PS as additives. The results showed that 0.8 wt% of ATP-PS had a great effect on the structure and performance of the membrane. With the increasing of the mass proportion of ATP-PS in the preparation of PPS base membrane, the microstructure of PPS based membrane was changed from blocky bicontinuous to spherical granular bicontinuous. When the addition amount of ATP-PS was 0.8 wt% of the total mass of PPS base membrane, PPS based membrane had strong hydrophobicity and organic solvent affinity, and its n-butanol flux could reach 106.9642 L m−2 h−1 bar−1. The rheological properties of PPS based membrane showed that ATP-PS was well compatible with the PPS, and ATP-PS was beneficial to crosslink between PPS molecular chains, thereby increasing the mechanical properties of PPS based membrane. Phase transition analysis demonstrated that ATP-PS (0.8 wt%) increased the melting temperature (2.34 °C) and crystallization temperature (2.63 °C) of PPS based membrane compared to PPS, thus allowing PPS to complete the phase transition at higher temperature interval during film formation, resulting in a stable microscopic cluster structure. Based on hydrophobic porous PPS membrane, PPS/ATP-PS/TA nanocomposites membrane with ATP-PS selective layer was prepared by co-deposition of tannic acid (TA) and ATP-PS on the surface of PPS membrane. The performance of PPS/ATP-PS/TA nanocomposites membrane was studied, which showed that the n-butanol flux of PPS/ATP-PS/TA nanocomposites membrane was 61.2913 L m−2 h−1 bar−1. More importantly, the simulated filtration performance of MB dye organic waste liquid (the solvent is n-butanol) showed that the maximum rejection rate of MB dye reached 99.82%. These results demonstrate that PPS/ATP-PS/TA nanocomposites membrane will have potential application in the filtration of organic dye wastewater.

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Abbreviations

PS:

Polystyrene

ATP:

Attapulgite

PPS:

Polyphenylene sulfide

ATP0:

Natural attapulgite

ATP-A:

Acidized attapulgite

ATP-K:

ATP-A grafted with KH570

ATP-PS:

ATP-K surface grafting polymerization PS

DBP:

Dibutyl phthalate

TIPS:

Thermally induced phase separation

TA:

Tannic acid

DA:

Dopamine

GA:

Gallic acid

MB:

Methylene blue

KH570:

γ-Methacryloxypropyltrimethoxysilane

TEM:

Transmission electronic microscopy

XPS:

X-ray photoelectron spectrometer

FTIR:

Fourier transform infrared spectrometer

T m :

Melting temperature

T c :

Crystallization temperature

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Acknowledgments

Financial support from the Key R&D project in Xinjiang Uygur Autonomous Region of China (2018B02016-3) is greatly acknowledged.

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  1. State Key Laboratory of Chemistry and Utilization of Carbon-Based Energy Resources, Key Laboratory of Oil and Gas Fine Chemicals, Ministry of Education and Xinjiang Uygur Autonomous Region, School of Chemical Engineering and Technology, Xinjiang University, Urumqi, 830017, China

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Li, C., Zhen, W. Preparation, performance and structure-properties relationship of polyphenylene sulfide/ATP-PS/co-deposition of tannic acid nanocomposites membrane. Polym. Bull. 81, 969–993 (2024). https://doi.org/10.1007/s00289-023-04748-y

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