Abstract
Additive manufacturing (AM) has advanced the manufacturing industry and has been employed in a wide range of industrial applications, including aerospace, automotive, medical, and die-casting equipment. To ensure the cost-effectiveness of the AM process, unfused powder must be recycled even if its characteristics may change after each cycle, making essential the validation of powder quality and component mechanical performances. Despite the research published to date, predicting the mechanical performance of printed parts issued from reused powder remains challenging since it is dependent on many AM process variables. Until now, no research has looked at the impact of powder recycling on the fatigue behavior of maraging steel components. This study investigates the impact of maraging steel powder reuse on powder characteristics, as well as on the tensile and fatigue properties of printed components. Our results indicate that the powder particle size distribution increased after eight powder reuses, particle morphology showed the presence of aggregates, broken particles, and shattered and deformed particles, while powder apparent density remained constant. Powder reusing had no significant impact on the surface roughness of as-built specimens. Although there was a slight decrease in mechanical properties over reuse cycles, tensile and fatigue performance remained globally stable, while the standard deviation of fatigue stress became narrower after eight cycles. Finally, fractography revealed that the fatigue fracture surfaces of components manufactured from an eight-time recycled powder have more fusion defects and carbon inclusions than the parts made from virgin powder.
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References
Diegel O, Nordin A, Motte D (2019) A practical guide to design for additive manufacturing. Springer
Powell D, Rennie AEW, Geekie L, Burns N (2020) Understanding powder degradation in metal additive manufacturing to allow the upcycling of recycled powders. J Clean Prod 268:122077. https://doi.org/10.1016/j.jclepro.2020.122077
Moghimian P et al (2021) Metal powders in additive manufacturing: a review on reusability and recyclability of common titanium, nickel and aluminum alloys. Addit Manuf 43:102017. https://doi.org/10.1016/j.addma.2021.102017
Popov VV, Katz-Demyanetz A, Garkun A, Bamberger M (2018) The effect of powder recycling on the mechanical properties and microstructure of electron beam melted Ti-6Al-4 V specimens. Addit Manuf 22:834–843. https://doi.org/10.1016/j.addma.2018.06.003
Brika SE, Letenneur M, Dion CA, Brailovski V (2020) Influence of particle morphology and size distribution on the powder flowability and laser powder bed fusion manufacturability of Ti-6Al-4V alloy. Addit Manuf 31:100929
Liu B, Wildman R, Tuck C, Ashcroft I, Hague R (2011) Investigation the effect of particle size distribution on processing parameters optimisation in selective laser. https://doi.org/10.26153/tsw/15290
Tang HP, Qian M, Liu N, Zhang XZ, Yang GY, Wang J (2015) Effect of powder reuse times on additive manufacturing of Ti-6Al-4V by selective electron beam melting. Jom 67(3):555–563. https://doi.org/10.1007/s11837-015-1300-4
Carrion PE, Soltani-Tehrani A, Phan N, Shamsaei N (2018) Powder recycling effects on the tensile and fatigue behavior of additively manufactured Ti-6Al-4V parts. Jom 71(3):963–973. https://doi.org/10.1007/s11837-018-3248-7
Quintana OA, Alvarez J, McMillan R, Tong W, Tomonto C (2018) Effects of reusing Ti-6Al-4V powder in a selective laser melting additive system operated in an industrial setting. Jom 70(9):1863–1869. https://doi.org/10.1007/s11837-018-3011-0
Park SB, Road B, Kingdom U (2016) Investigating the effects of multiple re-use of Ti6Al4V powder in additive manufacturing. Renishaw plc 1–10. [Online]. Available: www.renishaw.com
O’Leary R, Setchi R, Prickett P, Hankins G (2016) An investigation into the recycling of Ti-6Al-4V powder used within SLM to improve sustainability. InImpact J Innov Impact 8(2):377
Seyda V, Kaufmann N, Emmelmann C (2012) Investigation of aging processes of Ti-6Al-4 V powder material in laser melting. Phys Procedia 39:425–431. https://doi.org/10.1016/j.phpro.2012.10.057
Soundarapandiyan G et al (2021) The effects of powder reuse on the mechanical response of electron beam additively manufactured Ti6Al4V parts. Addit Manuf 46:102. https://doi.org/10.1016/j.addma.2021.102101
Alamos FJ et al (2020) Effect of powder reuse on mechanical properties of Ti-6Al-4V produced through selective laser melting. Int J Refract Met Hard Mater 91:105273. https://doi.org/10.1016/j.ijrmhm.2020.105273
Contaldi V, Del Re F, Palumbo B, Squillace A, Corrado P, Di Petta P (2019) Mechanical characterisation of stainless steel parts produced by direct metal laser sintering with virgin and reused powder. Int J Adv Manuf Technol 105(7–8):3337–3351. https://doi.org/10.1007/s00170-019-04416-4
Ahmed F et al (2020) Study of powder recycling and its effect on printed parts during laser powder-bed fusion of 17–4 PH stainless steel. J Mater Process Technol 278:116
Soltani-Tehrani A, Pegues J, Shamsaei N (2020) Fatigue behavior of additively manufactured 17–4 PH stainless steel: the effects of part location and powder re-use. Addit Manuf 36:101398
Jacob G, Brown CU, Donmez MA, Watson SS (2017). J Slotwinski. https://doi.org/10.6028/nist.Ams.100-6
Sutton AT, Kriewall CS, Karnati S, Leu MC, Newkirk JW (2020) Characterization of AISI 304L stainless steel powder recycled in the laser powder-bed fusion process. Addit Manuf 32:100981
Del Re F et al (2018) Statistical approach for assessing the effect of powder reuse on the final quality of AlSi10Mg parts produced by laser powder bed fusion additive manufacturing. Int J Adv Manuf Technol 97(5–8):2231–2240. https://doi.org/10.1007/s00170-018-2090-y
Asgari H, Baxter C, Hosseinkhani K, Mohammadi M (2017) On microstructure and mechanical properties of additively manufactured AlSi10Mg_200C using recycled powder. Mater Sci Eng, A 707:148–158. https://doi.org/10.1016/j.msea.2017.09.041
Yi F, Zhou Q, Wang C, Yan Z, Liu B (2021) Effect of powder reuse on powder characteristics and properties of Inconel 718 parts produced by selective laser melting. J Market Res 13:524–533. https://doi.org/10.1016/j.jmrt.2021.04.091
Rock C et al (2021) The influence of powder reuse on the properties of nickel super alloy ATI 718™ in laser powder bed fusion additive manufacturing. Metall and Mater Trans B 52(2):676–688. https://doi.org/10.1007/s11663-020-02040-2
Ardila LC et al (2014) Effect of IN718 recycled powder reuse on properties of parts manufactured by means of selective laser melting. Phys Procedia 56:99–107. https://doi.org/10.1016/j.phpro.2014.08.152
Sun H, Chu X, Liu Z, Gisele A, Zou Y (2021) Selective laser melting of maraging steels using recycled powders: a comprehensive microstructural and mechanical investigation. Metall and Mater Trans A 52(5):1714–1722. https://doi.org/10.1007/s11661-021-06180-1
Kim D et al (2020) Effect of heat treatment condition on microstructural and mechanical anisotropies of selective laser melted maraging 18Ni-300 steel. Metals 10(3):410. https://doi.org/10.3390/met10030410
Oliveira AR, Diaz JAA, Nizes ADC, Jardini AL, Del Conte EG (2021) Investigation of building orientation and aging on strength–stiffness performance of additively manufactured maraging steel. J Mater Eng Perform 30(2):1479–1489. https://doi.org/10.1007/s11665-020-05414-4
Gatto A, Bassoli E, Denti L (2018) Repercussions of powder contamination on the fatigue life of additive manufactured maraging steel. Addit Manuf 24:13–19. https://doi.org/10.1016/j.addma.2018.09.004
Horn M et al (2020) Influence of metal powder cross-contaminations on part quality in laser powder bed fusion: copper alloy particles in maraging steel feedstock. Procedia CIRP 94:167–172
E. G.-E. O. Systems, “EOS MaragingSteel MS1 DATA SHEET,” 2017. [Online]. Available: www.eos.info. Accessed 10.2017
Lutter-Günther M, Gebbe C, Kamps T, Seidel C, Reinhart G (2018) Powder recycling in laser beam melting: strategies, consumption modeling and influence on resource efficiency. Prod Eng Res Devel 12(3–4):377–389. https://doi.org/10.1007/s11740-018-0790-7
Raugel G, Yi Y (2015) Professor Klaus Kirchgässner. J Dyn Diff Equat 27(3–4):333–334. https://doi.org/10.1007/s10884-015-9497-z
Kriewall CS, Sutton AT, Karnati S, Leu MC, Newkirk JW (2020) Characterization of AISI 304L stainless steel powder recycled in the laser powder-bed fusion process. Addit Manuf 32:100981
Pal S et al (2021) The effects of locations on the build tray on the quality of specimens in powder bed additive manufacturing. Int J Adv Manuf Technol 112(3–4):1159–1170. https://doi.org/10.1007/s00170-020-06563-5
Astm I (2016) ASTM E8/E8M-16a: standard test methods for tension testing of metallic materials. ASTM International, West Conshohocken, PA, USA
ASTM (2015) Standard practice for conducting force controlled constant amplitude axial fatigue tests of metallic materials. https://doi.org/10.1520/E0466-15
A. f. d. n. (afnor) Essais de fatigue traitement statistique des données, A03-405, p 48, Septembre 1991
Ekaputra IMW, Dewa RT, Haryadi GD, Kim SJ (2020) Fatigue strength analysis of S34MnV steel by accelerated staircase test. Open Eng 10(1):394–400. https://doi.org/10.1515/eng-2020-0048
Dawes J, Bowerman R, Trepleton R (2015) Introduction to the additive manufacturing powder metallurgy supply chain. Johnson Matthey Technol Rev 59(3):243–256. https://doi.org/10.1595/205651315x688686
Pasebani S, Ghayoor M, Badwe S, Irrinki H, Atre SV (2018) Effects of atomizing media and post processing on mechanical properties of 17–4 PH stainless steel manufactured via selective laser melting. Addit Manuf 22:127–137. https://doi.org/10.1016/j.addma.2018.05.011
Snyder PM, Lu MW, Lee YL (2004) Reliability-based fatigue strength testing by the staircase method. SAE Technical Paper, 0148–7191
Scientifics S (2021) Brittle Fracture. Technical White Paper, p 6. [Online]. Available: surescreenscientifics.com
Szost B, Wang X, Johns D, Sharma S, Clare A, Ashcroft I (2018) Spatter and oxide formation in laser powder bed fusion of Inconel 718. Addit Manuf 24:446–456
Acknowledgements
The authors would like to express their appreciation for the support provided by Jonathan Coudé, Farhadipour Pedram, Karel J. Uhlir, Charles-André Fraser, Dany Morin, Richard Lafrance, and Loubert Suzie for their assistance during this project.
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This research was funded by NSERC, grant CDEPJ/507533.
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The novel ideas and work plan were established by Othmane Rayan and Jean Brousseau to meet the study objectives. Powder particles size, powder morphology, and fractography analysis were performed by Othmane Rayan, Claude Belzile, and Jonathan Coudé. The design, fabrication, and testing were performed by Othmane Rayan and Jean Brousseau. Abderazak El ouafi contributed to manuscript drafting and correcting. All authors read and approved the final manuscript.
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Rayan, O., Brousseau, J., Belzile, C. et al. Maraging steel powder recycling effect on the tensile and fatigue behavior of parts produced through the laser powder bed fusion (L-PBF) process. Int J Adv Manuf Technol 127, 1737–1754 (2023). https://doi.org/10.1007/s00170-023-11522-x
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DOI: https://doi.org/10.1007/s00170-023-11522-x