Abstract
In this paper, the strain-induced martensite transformation (SIMT) process of 304 stainless steel tubes under the action of a high shear stress state (HSSS) in the deformation zone of a new spinning process is studied and analyzes the changes in the microstructure and mechanical properties of each tubular workpiece obtained after continuous cold spinning under HSSS. Firstly, the contact equations and stress–strain state equations for the external cold extrusion spinning (ECES) were established and combined with the stress state criterion to find that ECES has a higher softening coefficient than conventional spinning (CS) in the deformation zone. To study the performance of the workpiece at each stage of processing, a longitudinal unidirectional tensile test was carried out on 304 stainless steel tubes. The material was obtained by cold spinning 5 times in succession for each pass of the tube, while X-ray diffraction (XRD) analysis was performed to measure the phase volume fraction of the workpiece at each stage, which provides a reference for subsequent transmission electron microscope (TEM) observation of the microstructure. The results show that the martensitic phase changes gradually after the volume fraction of martensite grows to a peak of 35% and gradually refines and fractures in tension, forming ultra-fine grain size laths of martensitic phase, while the tensile limit increases by 2.1 times, at which time the elongation at break is less than 5%.
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References
Talha M, Behera CK, Sinha OP (2013) A review on nickel-free nitrogen containing austenitic stainless steels for biomedical applications. Mat Sci Eng C-Mater 33:3563–3575. https://doi.org/10.1016/j.msec.2013.06.002
Chen AY, Ruan HH, Wang J, Chan HL, Wang Q, Li Q, Lu J (2011) The influence of strain rate on the microstructure transition of 304 stainless steel. Acta Mater 59:3697–3709. https://doi.org/10.1016/j.actamat.2011.03.005
Kishore K, Kumar RG, Chandan AK (2020) Critical assessment of the strain-rate dependent work hardening behaviour of AISI 304 stainless steel. Mater Sci Eng A-Struct 803:140675. https://doi.org/10.1016/j.msea.2020.140675
Lyamkin V, Pauly C, Starke P, Mucklich F, Boller C (2021) Impact of cyclic strain on deformation-induced martensite morphology and magnetic properties of type 347 austenitic stainless steel. Mater Today Commun 26:101803. https://doi.org/10.1016/j.mtcomm.2020.101803
Han BJ, Xu Zh (2007) Martensite phase transformation behavior of severe plastic deformed austentite at low temperature. J Iron Steel Res Int 19(80–83):88. https://doi.org/10.1002/jrs.1570
Cios G, Tokarski T, Zywczak A, Dziurka R, Stepien M, Gondek L, Marciszko M, Pawłowski B, Wieczerzak K, Bała P (2017) The investigation of strain-induced martensite reverse transformation in AISI 304 austenitic stainless steel. Metall Mater Trans A 48:4999–5008. https://doi.org/10.1007/s11661-017-4228-1
Renard K, Idrissi H, Schryvers D, Jacques PJ (2012) On the stress state dependence of the twinning rate and work hardening in twinning-induced plasticity steels. Scr Mater 66:966–971. https://doi.org/10.1016/j.scriptamat.2012.01.063
Santacreu PO, Glez JC, Chinouilh G, Frohlich T (2006) Behaviour model of austenitic stainless steels for automotive structural parts. Steels Autom Appl 77:9–10. https://doi.org/10.1002/srin.200606448
Mansourinejad M, Ketabchi M (2017) Modification of Olson-Cohen model for predicting stress-state dependency of martensitic transformation. Mater Sci Technol 33:1948–1954. https://doi.org/10.1080/02670836.2017.1342016
Kalpakcioglu S, Rajagopal S (1982) Spinning of tubes: a review. J Appl Metalwork 2:211–223. https://doi.org/10.1007/BF02834039
Matsuno KI (1997) Recent research and development in metal forming in Japan. J Mater Process Technol 66:1–3. https://doi.org/10.1016/S0924-0136(96)02139-5
Hayama M, Kudo H (1997) Theoretical study of tube spinning. Trans Jpn Soc Mech Eng 44:3286–3295. https://doi.org/10.1299/kikai1938.44.3286
Nahshon K, Hutchinson JW (2008) Modification of the Gurson model for shear failure. Eur J Mech A-Solids 27:1–17. https://doi.org/10.1016/j.euromechsol.2007.08.002
Gurson AL (1977) Continuum theory of ductile rupture by void nucleation and growth: part I—yield criteria and flow rules for porous ductile media. J Eng Mater Technol-Trans ASME 99:297–300. https://doi.org/10.1115/1.3443401
Xue L (2007) Ductile fracture modeling: theory, experimental investigation and numerical verification. Dissertation Mass Inst Technol. http://hdl.handle.net/1721.1/40876
Xu W, Zhao X, Ma H, Shan D, Lin H (2016) Influence of roller distribution modes on spinning force during tube spinning. Int J Mech Sci 113:10–25. https://doi.org/10.1016/j.ijmecsci.2016.04.009
Ma ZE (1993) Optimal angle of attack in tube spinning. J Mater Process Technol 37:217–224. https://doi.org/10.1016/0924-0136(93)90092-K
Li YY (2010) Research on lubrication technology of ferite stainless strip steel in tandem cold rolling. Northeast Univ. https://doi.org/10.1016/S1006-706X(15)60017-6
Huang HW, Wang ZB, Lu J, Lu K (2015) Fatigue behaviors of AISI 316L stainless steel with a gradient nanostructured surface layer. Acta Mater 87:150–160. https://doi.org/10.1016/j.actamat.2014.12.057
Shi Y, Wang Y, Shang W, Wang L, Zhang X, Liu H, Wang Y, Lv Zh, Sun Sh, Xu D (2021) Influence of grain size distribution on mechanical properties and HDI strengthening and work-hardening of gradient-structured materials. Mater Sci Eng A-Struct 811:141053. https://doi.org/10.1016/j.msea.2021.141053
He YM, Wang YH, Guo K, Wang TS (2017) Effect of carbide precipitation on strain-hardening behavior and deformation mechanism of metastable austenitic stainless steel after repetitive cold rolling and reversion annealing. Mater Sci Eng A-Struct 708:248–253. https://doi.org/10.1016/j.msea.2017.09.103
Liu T, Pan F, Zhang X (2013) Effect of Sc addition on the work-hardening behavior of ZK60 magnesium alloy. Mater Des 43:572–577. https://doi.org/10.1016/j.matdes.2012.07.050
Rodríguez-Martínez JA, Pesci R, Rusinek A (2011) Experimental study on the martensitic transformation in AISI 304 steel sheets subjected to tension under wide ranges of strain rate at room temperature. Mater Sci Eng A-Struct 528:5974–5982. https://doi.org/10.1016/j.msea.2011.04.030
Sharma S, Kumar BR, Kashyap BP, Prabhu N (2018) Effects of concurrent strain induced martensite formation on tensile and texture properties of 304L stainless steel of varying grain size distribution. MAT SCI ENG A-STRUCT 725:215–227. https://doi.org/10.1016/j.msea.2018.03.099
Remy L (1977) Kinetics of strain-induced fcc→hcp martensitic transformation. Metall Trans A 8:253–258. https://doi.org/10.1007/BF02661637
Das A, Chakraborti PC, Tarafder S, Bhandeshia HKDH (2011) Analysis of deformation induced martensitic transformation in stainless steels. Mater Sci Technol 27:366–370. https://doi.org/10.1179/026708310X12668415534008
Mansourinejad M, Ketabchi M (2017) Modification of modification of Olson-Cohen model for predicting stress-state dependency of martensitic transformation. M Mater Sci Technol. https://doi.org/10.1080/02670836.2017.1342016
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This work was supported by the Shanxi Coal Based Low Carbon Joint Fund (U1610118), National Key R&D Program of China (2018YFB1308701), National Natural Science Foundation of China (No. 51375325), and the Shanxi Provincial Special Fund for Coordinative Innovation Center of Taiyuan Heavy Machinery Equipment for their support to this research.
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All authors contributed to the study conception and design. Material preparation, data collection, and analysis were performed by Weizhuang Li, Wang Tian, and Guoqing Zhang. The first draft of the manuscript was written by Yiwei Xu, and all authors commented on the previous versions of the manuscript. All authors read and approved the final manuscript.
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Xu, Y., Li, W., Tian, W. et al. Microstructural evolution of external cold extrusion spinning 304 stainless steel with cumulative large deformation in multiple passes. Int J Adv Manuf Technol 123, 1009–1024 (2022). https://doi.org/10.1007/s00170-022-10107-4
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DOI: https://doi.org/10.1007/s00170-022-10107-4