Summary
Systematic TLC separations, identification of cations and the determination of the limits of their identification on microcrystalline cellulose layers, incorporating glyoxal dithiosemicarbazone (H2-GDTS) as a spray reagent have been worked out. Metal-GDTS complexes have also been separated on silica gel ‘G’ support. Detection called for no spray reagent, owing to the intense and characteristic colours of the complexes.
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References
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Johri, K.N., Venugopalan, K.A. & Arora, B.S. Glyoxal dithiosemicarbazone as a complexing and chromogenic spray reagent in inorganic TLC. Chromatographia 12, 476–478 (1979). https://doi.org/10.1007/BF02302994
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DOI: https://doi.org/10.1007/BF02302994