Abstract
A flavone glycoside was isolated from the leaves ofBetula platyphylla var.latifolia and chracterized as 4′,6-Dimethoxy-5-hydroxyflavone-7-O-β-D-glucoside(pectolinarigenin-7-O-β-D-glucopyranoside) by method of chemical and NMR spectral analysis.13C-1H long range coupling was confirmative for determination of its substituted position. In connection with this study, 6-C-Glucosylnalingenin and 6-C-Glucosylaromadendrin were confirmed its structures using this technique.
Similar content being viewed by others
References Cited
Bruno, M., Sanova, G., Lamartina, L., Lentini, F., New Flavonoids fromBonannia graeca.Heterocycles, 23, 1147–1153 (1985).
Harborne, J. B. and Mabry, T. J., The Flavonoids: Advances in Research. Chapman and Hall, New York, 1982.
Lee, M.-W., Flavonoids from the leaves ofBetula platyphylla var.latifolia.Kor. J. Pharmacog., 25, 199–203 (1994).
Lee, H.-B., Kwak, J.-H., Zee, O.-P. and Yoo, S.-J., Flavonoids from Cirsium rhinoceros.Arch. Pharm. Res., 17, 273–277 (1994).
Markham, K. R., Technique of Flavonoid Identification. Academic Press, New York, 1982.
Shirataki, Y., Yokoe, I., Endo, M. and Komatsu, M., Determination of C-6 or C-8 Substituted Flavanone Using13C-1H Long Range Coupling and the Revised Structures of Some Flavanone.Chem. Pharm. Bull., 33, 444–447 (1985).
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Lee, MW. Determination of the structure for polysubstituted flavonoid and 6-C-glucosyl flavonoids using13C-1H long range couplings. Arch. Pharm. Res. 17, 487–489 (1994). https://doi.org/10.1007/BF02979132
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF02979132