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Stereochemical studies of oligomers XXIX. Reinvestigation of the structure of N-m-tolyl phthalimide

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Abstract

C15H11NO2, Mr 237.3, monoclinic, space groupC c, a=8.539(2),b=19.865(4),c=7.599(2)Å,β=111.44(2)°,V=1199.8 Å3,Z=4,D c=1.31 gcm−3,λ(CuKα)=1.5418 Å,µ=6.74cm−1,F(000)=496, room temperature. The structure was solved by direct methods with SHELX-86 and refined down to agreement valueR=0.046 for 1117 reflections above 2σ(I). The angle between the plane of the phthalimide group, which shows a little bent [1.2(2)°] between its two rings, and the tolyl group is 56.1(1)°. The packing of the molecules is stabilized by van der Waal’s forces only.

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References

  • Allen F H and Trotter J 1971J. Chem. Soc. B1073

  • Belletti D, Cantoni A and Pasquinelli G 1988 Gestione on line di Diffrattometro a Cristallo Singolo Siemens AED con sistema IBM PS2/30. Centro di studio per la strutturistica diffrattometrica del C.N.R. Parma. Internal report 1/88

  • Bocelli G and Cantoni A 1989Acta Crystallogr. C45 1658

    Google Scholar 

  • Bocelli G and Rizzoli C 1990Acta Crystallogr. C46 2259

    Google Scholar 

  • Chandrasekhar K, Vasantha Pattabhi and Swaminathan S 1983Pramana J. Phys. 20 19

    Article  ADS  Google Scholar 

  • Ghosh M, Basak A K, Roy P N, Mazumdar S K and Sheldrick B 1987Acta Crystallogr. C43 732

    Google Scholar 

  • Hamilton W C 1959Acta Crystallogr. 12 609

    Article  Google Scholar 

  • Herbstein F H and Kaftor M 1981Z. Crystallogr. 157 1

    Google Scholar 

  • Lehmann M S and Larsen F K 1974Acta Crystallogr. A30 580

    ADS  Google Scholar 

  • Magomedova S, Dzybchenko A V, Zavodnik V E 1980Cryst. Struct. Commun. 9 713

    Google Scholar 

  • Magomedova S and Bel’skii V K 1986Krystallografiya 31 102

    Google Scholar 

  • Ribar B, Stankovic S, Herak R, Halasi R and Djuvic S 1974Cryst. Struct. Commun. 3 669

    Google Scholar 

  • Rizzoli C, Sangermano V, Calestani G and Andreetti G D 1987J. Appl. Crystallogr. 20 436

    Article  Google Scholar 

  • Sheldrick G M 1985 SHELX-86. InCrystallographic Computing 3, (eds) G M Sheldrick, C Kruger and R Goddard (Oxford: University Press)

    Google Scholar 

  • Ugozzoli F 1986Comput. Chem. 11(2) 109

    Article  Google Scholar 

  • Voliotis S, Arrieta J M and Germain G 1984Acta Crystallogr. C40 1946

    Google Scholar 

  • Walker M and Stuart D 1983Acta Crystallogr. A39 158

    Google Scholar 

Download references

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  1. Centre for Structural Diffractometry of C.N.R., Viale delle Scienze, I - 43100, Parma, Italy

    G Bocelli

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  1. G Bocelli
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Part XXVIII: Bocelli and Rizzoli (1990)

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Bocelli, G. Stereochemical studies of oligomers XXIX. Reinvestigation of the structure of N-m-tolyl phthalimide. Pramana - J Phys 36, 589–593 (1991). https://doi.org/10.1007/BF02845796

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  • DOI: https://doi.org/10.1007/BF02845796

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