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Reverse-phase liquid chromatography ofp-tert-butylcalixarenes

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Summary

Thep-tert-butylcalix[n]arenes (n=4,6,7,8) andp-tert-butyldihomooxacalix[4]arene have been separated by reverse phase liquid chromatography. Optimum conditions have been obtained on a Spherisorb ODS1, 5 µm C18 column by isocratic ambient elution with acetonitrile-methyltert-butyl ether. Calibration plots have been obtained from purified calixarenes and the reliability of the method is confirmed from test mixtures of calixarenes of known composition.

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Authors and Affiliations

  1. Laboratoire de Chimie Industrielle, Université Lyon 1, 43, boulevard du 11 Novembre 1918, 69622, Villeurbanne Cedex, France

    F. Vocanson, R. Lamartine, C. Duchamp & J. B. Regnouf de Vains

Authors
  1. F. Vocanson
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  2. R. Lamartine
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  3. C. Duchamp
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  4. J. B. Regnouf de Vains
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Vocanson, F., Lamartine, R., Duchamp, C. et al. Reverse-phase liquid chromatography ofp-tert-butylcalixarenes. Chromatographia 41, 204–206 (1995). https://doi.org/10.1007/BF02688026

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  • DOI: https://doi.org/10.1007/BF02688026

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