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Analogy of thermogravimetric measurements

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Abstract

Dimensionless number has been developed and introduced for quantitative analysis of the effect of thermogravimetric measuring factors like sample quantity, heating rate, etc. The TG, DTG and T data of different thermogravimetric measurements can be used directly for calculation of the three constants of analogy. TG data of CaCO3 measured in very different conditions show the method of transformation and its applicability for calculation of the correlation of measurements.

Zusammenfassung

Zur quantitativen Analyse des Effektes verschiedener Faktoren bei thermogravimetrischen Messungen wie z. B. Probenmenge, Aufheizgeschwindigkeit usw. wurde eine dimensionslose Zahl entwickelt und eingeführt. Die TG-, DTG- und T-Angaben verschiedener gravimetrischer Messungen können direct zur Berechnung der drei Vergleichskonstanten verwendet werden. Die unter verschiedenen Bedingungen gemessenen TG-Daten für CaCO3 zeigen die Transformationsmethode und ihre Anwendbarkeit für die Berechnung der Korrelation der Messungen.

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Adonyi, Z. Analogy of thermogravimetric measurements. Journal of Thermal Analysis 42, 491–503 (1994). https://doi.org/10.1007/BF02548531

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