Skip to main content
Log in

A rapid chemical separation procedure for the determination of burn-up of nuclear fuel

  • Published:
Journal of Radioanalytical Chemistry Aims and scope Submit manuscript

Abstract

A chemical separation procedure for the determination of burn-up is described. The isolation of uranium, plutonium and neodymium is based on two ion-exchange separations, the first one an anion exchange in hydrochloric acid—nitric acid medium and the second one a cation exchange under high pressure with α-hydroxyisobutyric acid. Several experimental facts like chemical yields, contaminations and cross contaminations are discussed.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. W. B. BREMNER, D. G. McROBERTS, Proc. Conf. on Nuclear Mass Spectrometry, Petten, October 1978, in preparation.

  2. H. QURESHI, E. LARSEN, L. TURI, J. OLSEN, J. HOUGAARD, Proc. IAEA Symp. on Analytical Methods in the Nuclear Fuel Cycle, IAEA-SM-149/13, November 1971.

  3. L. KOCH, T. MOY, D. STEINERT, Radiochim. Acta, 19 (1973) 94.

    CAS  Google Scholar 

  4. A. J. FUDGE, E. FORSTER, AERE-R-5309, 1966.

  5. S. F. MARSH, 155th ACS National Meeting, San Francisco, California, USA, April 1968.

  6. P. de REGGE, R. BODEN, J. Radioanal. Chem., 35 (1977) 173.

    Article  Google Scholar 

  7. B. F. RIDER, C. P. RUIZ, J. P. PETERSON, Jr., F. R. SMITH, GEAP-5354, October 1967.

  8. ASTM Standard, Part 30, Method E 321-69. American Society of Testing and Materials, Philadelphia, 1973, p. 1096.

  9. S. F. MARSH, M. R. ORTIZ, R. M. ABERNATHEY, J. E. REIN, LA-5567, June 1974.

  10. L. KOCH, A. CRICCHIO, F. GERIN, Proc IAEA Symp. on Analytical Methods in the Nuclear Fuel Cycle, IAEA-SM-149/2, November 1971.

  11. D. O. CAMPBELL, J. Inorg. Nucl. Chem. 35 (1973) 3911.

    Article  CAS  Google Scholar 

  12. S. M. QUAIM, Radiochem. Radioanal. Letters, 25 (1976) 335.

    Google Scholar 

  13. N. R. LARSEN, W. B. PEDERSEN, J. Radioanal. Chem., 45 (1978) 135.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

van Raaphorst, J.G., Haremaker, H. A rapid chemical separation procedure for the determination of burn-up of nuclear fuel. J. Radioanal. Chem. 53, 71–80 (1979). https://doi.org/10.1007/BF02517907

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02517907

Keywords

Navigation