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Determination of phenolic compounds from oxidation of lignin lake sediments by high-performance liquid chromatography

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Summary

An isocratic high-performance liquid chromatography method for the analysis of phenolic aldehydes, ketones and acids produced from the alkaline oxidation of lignin by CuO is described. The validated method was used for quantitation of lignin degradation phenols in a sediment core (450 cm) of the Infernão Lake (an oxbow lake of the Moji-Guaçu River, São Paulo, Brazil) to reconstruct paleoenvironmental changes responsible for the formation of this lake.

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Author notes

  1. I. Lobo

    Present address: Departmento de Química, Universidade Estadual de Londrina, Caixa Postal 6001, 86051-990, Londrina, PR, Brazil

Authors and Affiliations

  1. Laboratórios de Biogeoquímica Ambiental, Universidade Federal de Sāo Carlos, Caixa Postal 676, 13.565-905, Sāo Carlos, SP, Brazil

    I. Lobo & A. A. Mozefo

  2. Síntese Orgânica e CLAE Departamento de Química, Universidade Federal de Sāo Carlos, Caixa Postal 676, 13.565-905, Sāo Carlos, SP, Brazil

    Q. B. Cass

Authors
  1. I. Lobo
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  2. A. A. Mozefo
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  3. Q. B. Cass
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Lobo, I., Mozefo, A.A. & Cass, Q.B. Determination of phenolic compounds from oxidation of lignin lake sediments by high-performance liquid chromatography. Chromatographia 52, 727–731 (2000). https://doi.org/10.1007/BF02490996

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  • DOI: https://doi.org/10.1007/BF02490996

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