Summary
The etching of soda glass by hydrogen chloride has been studied by determining the weight of sodium chloride per unit area on single and double statically-etched glass. The influence of three coating solvents on the critical surface tension of etched and unetched glass has been determined by measuring the contact angles of a wide range of stationary phases. The dynamic coating procedure has been critically examined and certain aspects which lead to the production of improved columns are explored.
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References
J. L. Marshall andD. A. Parker, J. Chromatogr.122, 425 (1976).
K. Tesarik andM. Novotny inH. G. Struppe (Editor), Gas Chromatographie 1968, Akademic-Verlag, Berlin, p. 575.
G. Alexander, G. A. F. M. Rutten, Chromatographia6, 231 (1974).
G. Alexander, G. Garzo andG. Palyi, J. Chromatogr.91, 25 (1974).
G. Alexander andG. A. F. M. Rutten, J. Chromatogr.99, 81 (1974).
J. J. Franken, G. A. F. M. Rutten andJ. A. Rijks, J. Chromatogr.126, 117 (1976).
R. E. Johnson andR. H. Dettre in Contact Angle, Wettability and Adhesion, Advances in Chemistry Series No. 43, p. 112. Published by American Chemical Society, 1964.
J. Bouche andM. Verzele, J. Gas Chromatogr.6, 501 (1968).
F. Fairbrother andA. E. Stubbs, J. Chem. Soc.527 (1935).
G. Schomburg andH. Husmann, Chromatographia8, 517 (1975).
D. H. Desty, J. N. Haresnape andB. H. F. Whyman, Anal. Chem.32, 302 (1960).
J. A. Hockey andB. A. Pethica, Trans. Faraday Soc.57, 247 (1961).
J. Erkelens andB. G. Linsen, J. Coll. Inter. Sci.29, 464 (1969).
J. M. Bather andR. A. C. Gray, J. of Chromatogr.122, 159 (1976).
W. A. Zisman in Contact Angle, Wettability and Adhesion, Advances in Chemistry Series No. 43, p. 1. Published by American Chemical Society, 1964.
F. London, Trans. Faraday Soc.33, 8 (1937).
F. M. Fowkes in Contact Angle, Wettability and Adhesion, Advances in Chemistry Series No. 43, p. 40. Published by American Chemical Society, 1964.
K. D. Bartle andM. Novotny, J. Chromatogr.96, 35 (1974).
H. W. Fox, E. F. Hare andW. A. Zisman, J. Phys. Chem.59, 1097 (1955).
H. W. Fox, E. F. Hare andW. A. Zisman, J. Coll. Sci.8, 194 (1953).
G. Guiochon, J. Chromatogr. Sci.9, 512 (1971).
R. Kaiser, “Gas Phase Chromatography, Vol. II, Capillary Chromatography” Butterworths, London, 1963, p. 45.
M. Novotny, L. Blomberg andK. D. Bartle, J. Chromatogr. Sci.8, 390 (1970).
Saito andO. Furukawa, Bunseki Kagaku23, 339 (1974).
S. L. Goren, J. Fluid Mech.12, 309 (1962).
L. S. Ettre, Open Tubular Columns in Gas Chromatography, Plenum Press, New York, 1965, p. 15.
H. L. Goldsmith andS. G. Mason, J. Coll. Sci.18, 237 (1963).
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Parker, D.A., Marshall, J.L. Some investigations into the coating of glass open-tube columns. Chromatographia 11, 526–533 (1978). https://doi.org/10.1007/BF02311076
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DOI: https://doi.org/10.1007/BF02311076