Summary
The optimisation of chromatographic parameters is studied. The Window Diagram and Overlapping Resolution Map (ORM) methods are compared. The latter is developed to take into account the spot diameter and the average plate height variations with the development distance, in order to improve the reliability of the method.
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References
D. Nurok, Chem. Rev.,2, 363 (1989).
H. J. Issaq, J. R. Klose, K. L. McNitt, J. E. Haky, G. M. Muschik, J. Liq. Chromatogr.,4, 2091 (1981).
C. K. Bayne, C. Y. Ma, J. Liq. Chromatogr.,12, 235 (1989).
A. Zlatkis, R. E. Kaiser, (Ed.), HPTLC, J. Chromatogr. Library,9, 15–34 (1977).
F. Geiss, Fundamentals of Thin Layer Chromatography. Heidelberg, Basel, New York, Hütig (1987).
J. L. Glajch, J. J. Kirkland, K. N. Squire, J. M. Minor, j. Chromatogr.,199, 57 (1980).
J. L. Glajch, J. C. Gluckman, J. G. Charikofsky, J. M. Minor, J. J. Kirkland, J. Chromatogr.,318, 23 (1985).
C. P. Ong, H. K. Lee, S. F. Y. Li, J. Chromatogr.,464, 405 (1989).
S. F. Y. Li, H. K. Lee, C. P. Ong, J. Chromatogr.,506, 245 (1990).
Q. S. Wang, R. Y. Gao, H. Y. Wang, B. W. Yan, Chinese J. Chem.,9, 223 (1991).
Q. S. Wang, Z. P. Zhan, C. X. Wang, J. Planar Chromatogr.,4, 442 (1991).
R. E. Tecklenburg, Jr., G. H. Fricke, D. Nurok, J. Chromatogr.,290, 75 (1984).
Q. S. Wang, H. Y. Wang, J. Planar Chromatogr.,3, 15 (1990).
C. F. Poole, S. K. Poole, Anal. Chem.,61, 22, 1257 A (nov. 15 1989).
R. J. Laub, J. H. Purnell, J. Chromatogr.,112, 71 (1975).
A.-M. Siouffi, J. Chromatogr.,556, 81 (1991).
L. R. Snyder Principles of Adsorption Chromatography, Marcel Dekker: New York (1968).
B. Belenkii, O. Kurenbin, L. Litvinova, E. Gankina, J. Planar Chromatogr.,3, 340 (1990).
G. Guiochon, A. Siouffi, J. Chromatogr. Sci.,16, 470 (1978).
G. Guiochon, F. Bressolle, A. Siouffi, J. Chromatogr. Sci.,17, 368 (1979).
C. L. de Ligny, A. G. Remijnse, J. Chromatogr.,33, 242 (1968).
C. L. de Ligny, A. G. Remijnse, J. Chromatogr.,35, 257 (1968).
C. L. de Ligny, E. C. M. Kok, J. Chromatogr.,35, 268 (1968).
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Cavalli, E., Truong, T.T., Thomassin, M. et al. Comparison of optimization methods in planar chromatography. Chromatographia 35, 102–108 (1993). https://doi.org/10.1007/BF02278565
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DOI: https://doi.org/10.1007/BF02278565