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The effect of surface treatments of glass capillaries on column performance

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Summary

The effects of etching and/or silylation of glass capillaries on column efficiency were studied. Coated with apolar OV-101, only columns subjected to the combined treatment showed an increase of about 50% in the number of effective plates. Surface hydroxylation, prior to silylation, gave a small additional improvement for this stationary phase.

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Authors and Affiliations

  1. Laboratory for Instrumental Analysis, Eindhoven University, Eindhoven, Holland

    M. H. J. van Rijswick

  2. Institute for Instrumental Analytical Chemistry, Czechoslovak Academy of Sciences, Brno, Czechoslovakia

    K. Tesařík

Authors
  1. M. H. J. van Rijswick
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  2. K. Tesařík
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van Rijswick, M.H.J., Tesařík, K. The effect of surface treatments of glass capillaries on column performance. Chromatographia 7, 135–137 (1974). https://doi.org/10.1007/BF02269824

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  • DOI: https://doi.org/10.1007/BF02269824

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