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Determination of the ultra long range spin-spin coupling constants using overall line shape analysis in the1H NMR spectra of fullerene-C60 cycloadducts with 1-(4-nitrophenyl)-3-phenylnitrile ylide

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Abstract

On the basis of the overall signal line shape in the1H NMR spectra of [6,6]-closed and [5,6]-open fullerene-C60 cycloadducts with 1-(4-nitrophenyl)-3-phenylnitrile ylide we determined the values of the long range spin-spin coupling for the aliphatic proton of the heterocyclic fragment with the aromatic protons.

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M. V. Lomonosov State University, Moscow 119899, Russia. Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, pp. 1500–1505, November, 1999.

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Chertkov, V.A., Zubkov, S.V., Ovcharenko, A.A. et al. Determination of the ultra long range spin-spin coupling constants using overall line shape analysis in the1H NMR spectra of fullerene-C60 cycloadducts with 1-(4-nitrophenyl)-3-phenylnitrile ylide. Chem Heterocycl Compd 35, 1308–1312 (1999). https://doi.org/10.1007/BF02251999

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  • DOI: https://doi.org/10.1007/BF02251999

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