Skip to main content
Log in

Loss of elements in the oxygen flask decomposition of biological materials: A study by neutron activation analysis

  • Published:
Journal of Radioanalytical and Nuclear Chemistry Aims and scope Submit manuscript

Abstract

Partial loss of elements in the oxygen flask method for the decomposition of biological materials is described. The irradiated sample is placed in a platinum wire gauze or quartz cup and burnt in an oxygen atmosphere in the presence of carrier solutions. The results obtained by radiochemical neutron activation analysis for the elements like Mn, As, Cu, Sb and Zn in different standard reference materials are presented with a discussion of the possible causes for the lower values.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. R. E. THIERS, Separation, Concentration and Contamination in Trace Analysis, J. H. YOE, H. J. KOCH Jr. (Eds), Wiley & Sons. Inc., New York, 1957, p. 637.

    Google Scholar 

  2. P. W. WEST, Anal. Chem., 26 (1954) 121.

    Google Scholar 

  3. W. SCHÖNIGER, Z. Anal. Chem., 181 (1961) 28.

    Google Scholar 

  4. H. H. TAUSSKY, A. WASHINGTON, E. ZUBILLAGE, A. T. MILHORAT, Mikrochem. J., 10 (1966) 470.

    Google Scholar 

  5. A. M. G. MACDONALD, Advances in Analytical Chemistry and Instrumentation, C. N. REILLEY (Ed.), Vol. 4, Wiley & Sons, Inc., New York, 1965, p. 75.

    Google Scholar 

  6. J. BASSETT, R. C. DENNY, G. H. JEFFERY, J. MENDHAM, Vogel's Textbook of Quantitative Inorganic Analysis, 4th ed., The English Language Book Society and Longman, London, 1978, p. 115.

    Google Scholar 

  7. R. BOCK, I. L. MARR, A Handbook of Decomposition Methods in Analytical Chemistry, Halsted Press, 1979.

  8. J. RUŽIČKA, C. G. LAMM, Talanta, 16 (1969) 157.

    Google Scholar 

  9. T. T. GORSUCH, International Series of Monographs in Analytical Chemistry, Vol. 39, Pergamon Press, Oxford, 1970.

    Google Scholar 

  10. A. R. BYRNE, L. KOSTA, V. RAVNIK, J. STUPAR, V. HUDNIK, IAEA-SM-227/45, p. 2

  11. H. S. DANG, H. B. DESAI, D. D. JAISWAL, S. R. KAYASTH, S. SOMASUNDARAM, J. Radioanal. Chem., 77 (1983) 65.

    Google Scholar 

  12. R. BELCHER, A. M. G. MACDONALD, Talanta, 1 (1958) 408.

    Google Scholar 

  13. A. P. TERNTEV, S. I. OBTAMPERANSKAYA, V. N. LIKHOSHERSTOVA, Zh. Anal. Khim., 15 (1960) 748.

    Google Scholar 

  14. W. H. GUTENMANN, L. E. SAINT-JOHN, D. L. BARRY, E. D. JONES, D. J. LISK, J. Agr. Food. Chem., 9 (1961) 50.

    Google Scholar 

  15. HENG-BIN HAN, C. KAISER, G. TOLG, Anal. Chim. Acta, 128 (1981) 9.

    Google Scholar 

  16. Pure and Appl. Chem., 51 (1979) 1183.

  17. R. A. NADKARNI, G. H. MORRISON, J. Radioanal. Chem., 43 (1978) 347.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Desai, H.B., Kayasth, S.R., Parthasarathy, R. et al. Loss of elements in the oxygen flask decomposition of biological materials: A study by neutron activation analysis. Journal of Radioanalytical and Nuclear Chemistry, Articles 84, 123–127 (1984). https://doi.org/10.1007/BF02038187

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02038187

Keywords

Navigation