Abstract
The neutron activation method has been applied to the determination of Ag, Cd, Co, Cr, Cu, Fe, Hg, Mo, Se and Zn in waters and wastes. The method involves decomposition of organic substances by ozonation, preconcentration of elements to be determined by coprecipitation with thionalide at pH 9 or sorption on Dowes 1×2 loaded with 8-hydroxyquinoline-5-sulfonic acid at pH 7, irradiation of the concentrate, radiochemical separation of the respective radioisotopes and gamma spectrometric measurement of the activity. Accuracy and precision of the determination have been evaluated.
Similar content being viewed by others
References
N. KAHRMAN, I. ÖLMEZ, F. PAMUK, Measurement, Detection and Control of Environmental Pollutants, IAEA, Vienna 1976, p. 427.
A. KABATA-PENDIAS, H. PENDIAS, Trace Elements in the Biological Environment (in Polish), Wydawnictwo Geologiczne, Warsaw, 1979.
H. J. M. BOWEN, Environmental Chemistry of the Elements, Academic Press, London, 1979.
J. SCHNEIDER, R. GEISLER, Z. Anal. Chem., 267 (1973) 270.
E. HEUSS, K. H. LIESER, J. Radioanal. Chem., 50 (1979) 289.
T. BRAUN, A. B. FARAG, M. P. MALONEY, Anal. Chim. Acta, 93 (1977) 191.
G. L. JEWETT, R. P. HIMES, O. U. ANDERS, J. Radioanal. Chem., 37 (1977) 813.
S. GOHDA, Bull. Chem. Soc. Japan, 45 (1972) 1704.
T. FUJINAGA et al., J. Radioanal. Chem., 13 (1973) 301.
M. H. YANG, P. Y. CHEN, C. L. TSENG, S. J. YEH, P. S. WENG, J. Radioanal. Chem., 37 (1977) 801.
Y. KUSAKA, H. TSUJI, Y. TAMARI, T. SAGAWA, S. OKUORI, S. IMAI, T. OZAK, J. Radioanal. Chem., 37 (1977) 917.
C. BERGERIEUX, J. P. BLANC, W. HAERDI, J. Radioanal. Chem. 37 (1977) 823.
C. LEE, N. B. KIM, I. C. LEE, K. S. CHUNG, Talanta, 24 (1977) 241.
W. ZMIJEWSKA, H. POLKOWSKA-MOTRENKO, H. STOKOWSKA, to be published.
W. ZMIJEWSKA, H. POLKOWSKA-MOTRENKO, H. STOKOWSKA, J. Radioanal. Chem., 84 (1984) 319.
W. ZMIJEWSKA, H. POLKOWSKA-MOTRENKO, H. STOKOWSKA, Radiochem. Radioanal. Letters, 59 (1983) 337.
L. PSZONICKI, A. VEGLIA, O. SUCHNY, Report on Intercomparison W-3/1 of the Determination of Trace Elements in Water, IAEA, Vienna, 1982.
L. MART, Z. Anal. Chem., 296 (1979) 350.
H. KAISER, Z. Anal. Chem., 296 (1968) 80.
J. OP de BEECK, A Programme for Complete Quantitative Neutron Activation Analysis using Ge(Li) Detector Gamma Spectrometry and a Small Computer, Institute of Nuclear Sciences, Ghent University, Ghent.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Żmijewska, W., Polkowska-Motrenko, H. & Stokowska, H. Neutron activation analysis of water and waste. Journal of Radioanalytical and Nuclear Chemistry, Articles 116, 243–252 (1987). https://doi.org/10.1007/BF02035768
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF02035768