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Preparation, spectral studies and X-ray crystal structure of 1,3,5-triphenyl-1,5-pentanedione, C23H20O2

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Abstract

1,3,5-triphenyl-1,5-pentanedione, C23H20O2, has been prepared and characterized by spectroscopic methods and single crystal X-ray analysis. Crystals are monoclinic, space groupP21/n, a=28.124(4),b=5.997(1),c=10.434(1)Å, β-98.42(1)Å,Z=4. The structure has been refined to a finalR-value of 0.040 for 1625 reflections withF o>3σ(F o). The compound contains the two carbonyl groups in a mutuallycis arrangement.

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References

  1. Das, G.C., M. Sc. Thesis, Univ. of Dhaka, 1989.

  2. Rahman, M.T.; Das, G.C.; Halder, D.C.; Bahar, M.H.; Olsson, T.J. Chem. Soc., Perkin Trans. II, submitted for publication, 1994.

  3. Latif, K.A.; Adhikari, S.K.; Eunus, M.M.,J. Indian Chem. Soc. 1959a,36, 212.

    Google Scholar 

  4. Latif, K.A.; Razzaq, M.A.; Adhikari, S.K.; Eunus, M.M.,J. Indian Chem. Soc. 1959b,36, 209.

    Google Scholar 

  5. Jones, R. A.; Hursthouse, M.B.; Malik, K.M.A.; Wilkinson, G.J. Am. Chem. Soc. 1979,101, 4128.

    Google Scholar 

  6. Sheldrick, G.M. SHELX-86 program for crystal structure solution.Acta Crystallogr. 1990,A46, 467.

    Google Scholar 

  7. Sheldrick, G.M..SHELX-80 Program for Crystal Structure Determination: University of Gottingen, Germany

  8. Davies, K.. SNOOPI Program for Drawing Molecular and Crystal Structure; University of Oxford: England, 1983.

    Google Scholar 

  9. Allen, F.H.; Kennard, O.; Watson, D.G.; Brammer, L.; Orpen, A.G.; Taylor, R..J. Chem. Soc. Perkin Trans. 1987,II, S1-S19.

    Google Scholar 

  10. Jia, Z.; Quail, J.W.; Arora, V.K.; and Dimmock, J.R.Acta Crystallogr. 1989,C45, 1117.

    Google Scholar 

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Authors and Affiliations

  1. Department of Chemistry, University of Dhaka, 1000, Dhaka, Bangladesh

    G. C. Das, M. M. Rahman & M. T. Rahman

  2. School of Chemistry and Applied Chemistry, University of Wales Cardiff, P.O. Box 912, CF1 3TB, Cardiff, U.K.

    M. B. Hursthouse & K. M. A. Malik

  3. Department of Organic Chemistry, Chalmers University of Technology, S-41296, Göteborg, Sweden

    T. Olsson

Authors
  1. G. C. Das
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  2. M. B. Hursthouse
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  3. K. M. A. Malik
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  4. M. M. Rahman
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  5. M. T. Rahman
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  6. T. Olsson
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Das, G.C., Hursthouse, M.B., Malik, K.M.A. et al. Preparation, spectral studies and X-ray crystal structure of 1,3,5-triphenyl-1,5-pentanedione, C23H20O2 . J Chem Crystallogr 24, 511–515 (1994). https://doi.org/10.1007/BF01666729

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  • DOI: https://doi.org/10.1007/BF01666729

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