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Direct N-alkylation of carbonic acid amides by use of palladium catalyst complexes

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

Aromatic amides react with butadiene in the presence of Pd(acac)2-Ph3P-AlEt3 (1:3:4) in DMF, and aliphatic amides react with the diene in the presence of Pd(acac)2-Ph3P-CO2-NH2 (1:10:192:438) in N-methylpyrrolidone-2 to form primarily N-2,7-octadienylamides.

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Literature cited

  1. R. M. Safuanova, R. N. Fakhretdinov, and U. M. Dzhemilev, Izv. Akad. Nauk SSSR, Ser. Khim., 703 (1984).

  2. R. V. Kunakova and V. V. Sidorova, Proc. All-Union Conf. Metalloorg. Chem., Part 2, Ufa (1985), p. 232.

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Authors and Affiliations

  1. Institute of Chemistry, Bakshir Branch, Academy of Sciences of the USSR, Ufa

    R. M. Safuanova, R. N. Fakhretdinov & U. M. Dzhemilev

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  1. R. M. Safuanova
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  2. R. N. Fakhretdinov
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  3. U. M. Dzhemilev
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 4, pp. 821–828, April, 1988.

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Safuanova, R.M., Fakhretdinov, R.N. & Dzhemilev, U.M. Direct N-alkylation of carbonic acid amides by use of palladium catalyst complexes. Russ Chem Bull 37, 703–708 (1988). https://doi.org/10.1007/BF01455481

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  • DOI: https://doi.org/10.1007/BF01455481

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