Abstract
The compaction of thin-walled potcore compacts (height 10 mm, diameter 15 mm, wall thickness 1 mm) with a high homogeneity is analysed. High homogeneity implies that the density is uniform throughout the compact. In order to attain this goal, internal and external friction are minimized while the mode of pressing and pressing velocity are optimized. Internal friction refers to friction between the powder particles, which is influenced by the particle size distribution and additives. The use of five different additives is evaluated. External friction relates to the friction between the powder and the die wall, which is influenced by the relative hardness of the die wall and lubricants. The effects of three different coatings and a lubricant on friction with the die wall have been investigated. The homogeneity of compacts with complicated shapes is affected by the formation of large local density gradients, which lead to differential shrinkage during sintering. By characterizing the shape of sintered products, it is shown that the inhomogeneity in compacts is reduced by optimizing the pressing mode and the pressing velocity. This improves the variation of the diameter over the height of the sintered potcores from 3 to 1.0%
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References
A. Broese van Groenou, in “Ceramic monographs — handbook of ceramics”, supplement ofInterceram 31 (1982) pp. 1–10.
K. Masters, “Spray drying handbook” (George Godwin, London, 1985).
J. T. Fell andJ. M. Newton,J. Pharmacol. Sci. 59 (1970), 688.
A. S. James, W. M. Dawson andT. J. Davies,Powder Metall. 30 (1987) 267.
R. H. Marion andJ. K. Johnstone,Ceram. Bull. 56 (1977) 998.
K. Kendall andN. McAlford, inBrit. Ceram. Proc. 37 “Special ceramics 8” (Institute of Ceramics, Stoke an Trent, 1986).
M. Takahashi andS. Suzuki, in “Handbook of ceramics and composites”, edited by N. Cheremisinoff (Marcel Dekker, New York, 1990).
DIN 30911: Sintered metal materials-Sinter test procedures part 2: Determination of radial crushing strength (Benth Verlag GmbH, Berlin).
G. L. Messing, C. J. Markhoff andL. G. McCoy,Ceram. Bull. 61 (1982) 857.
R. L. Matsumoto,J. Amer. Ceram. Soc. 69 (1986) C-246.
H. J. Glass andG. de With,Powder Technol. submitted.
S. Strijbos,Powder Technol. 18 (1977) 209.
W. van Duyn andB. VAN Lochem,Thin Solid Films 8 (1989) 497.
R. Mallender, C. Dangerfield andD. Coleman,Powder Metall. 15 (1972) 130.
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Glass, H.J., de With, G., de Graaf, M.J.M. et al. Compaction of homogeneous (Mn, Zn)-ferrite potcores. J Mater Sci 30, 3162–3170 (1995). https://doi.org/10.1007/BF01209232
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DOI: https://doi.org/10.1007/BF01209232