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Synthesis and reactions of oxygen-containing organosilicon compounds Communication 5. Synthesis and reactions of aliphatic-aromatic silanediols

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Summary

  1. 1.

    It was shown that the dichloromethyl-1-naphthylsilane obtained by the organomagnesium method contains bromochloromethyl-1-naphthylsilane as impurity.

  2. 2.

    The procedure for preparing pure arylalkyldichlorosilanes was improved.

  3. 3.

    Conditions were found for the preparation of alkylarylsilanediols in the pure state by the hydrolysis of alkylaryldihalosilanes.

  4. 4.

    The following substances were prepared and characterized for the first time. methyl-1-naphthylsilanediol, ethyl- 1-naphthylsilanediol, dichloroethyl-1-naphthylsilane, chloroethyldi-1-naphthylsilane, chloromethyldi-1-naphthylsilane, the dibutyl ether of methyl-1-naphthylsilanediol, and the diacetic ester of methyl-1-naphthylsilanediol.

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Authors and Affiliations

  1. N. D. Zelinsky Institute of Organic Chemistry of the Academy of Sciences of the USSR, USSR

    M. F. Shostakovsky & Kh. I. Kondratyev

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  1. M. F. Shostakovsky
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  2. Kh. I. Kondratyev
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Shostakovsky, M.F., Kondratyev, K.I. Synthesis and reactions of oxygen-containing organosilicon compounds Communication 5. Synthesis and reactions of aliphatic-aromatic silanediols. Russ Chem Bull 5, 985–991 (1956). https://doi.org/10.1007/BF01166414

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  • DOI: https://doi.org/10.1007/BF01166414

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