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Crystal structure and IR spectra of the molecular complex of 5,6,7,8-tetrahydroquinoline with pentachlorophenol

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Abstract

The crystal structure of the molecular complex of 5,6,7,8-tetrahydroquinoline with pentachlorophenol (THQ PCP) has been solved by direct methods and refined toR=0.040 for 1981 nonzero independent reflections. The O-H⋯N hydrogen bridge is characterized by a 2.602(4) ÅO⋯N distance. The broad protonic absorption spread in the 500–3000 cm−1 range, with two intense submaxima at 900 and 2380 cm−1, shows relatively strong hydrogen bonds.

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References

  • Guissani, Y., and Ratajczak, H. (1981)Chem. Phys. 62, 319–331.

    Google Scholar 

  • International Tables for X-Ray Crystallography (1974) Vol. IV (Kynoch Press, Birmingham).

  • Janoschek, R., Weidemann, E. G., Pfeiffer, H., and Zundel, G., (1972)J. Amer. Chem. Soc. 94, 2387–2396.

    Google Scholar 

  • Majerz, I., Malarski, Z., and Lis, T. (1987)J. Mol. Struct. 161, 165–173.

    Google Scholar 

  • Majerz, I., Malarski, Z., and Lis, T. (1988)Bull. Pol. Acad. Sci. Chem. 36, 151–157.

    Google Scholar 

  • Majerz, I., Malarski, Z., and Lis, T. (1989a)J. Mol. Struct. 213, 161–168.

    Google Scholar 

  • Majerz, I., Malarski, Z., and Lis, T. (1989b)Bull. Pol. Acad. Sci. Chem. 37, 81–89.

    Google Scholar 

  • Majerz, I., Malarski, Z., and Lis, T. (1989c)J. Crystallogr. Spectr. Res. 19, 349–356.

    Google Scholar 

  • Majerz, I., Malarski, Z., and Lis, T. (1990)J. Mol. Struct. 240, 47–58.

    Google Scholar 

  • Malarski, Z., Majerz, I., and Lis, T. (1987a)Acta Crystallogr. C43, 1766–1769.

    Google Scholar 

  • Malarski, Z., Majerz, I., and Lis, T. (1987b)J. Mol. Struct. 158, 369–377.

    Google Scholar 

  • Onda, M., and Yamaguchi, I. (1978)Bull. Chem. Soc. Jpn. 51, 3121–3124.

    Google Scholar 

  • Pedersen, T., Larsen, N. W., and Nygaard, L. (1969)J. Mol. Struct. 4, 59–77.

    Google Scholar 

  • Romanowski, H., and Sobczyk, L. (1977)Chem. Phys. 19, 361–370.

    Google Scholar 

  • Sheldrick, G. M., (1976)Shelx 76,Program for crystal structure determination, University of Cambridge.

  • Sobczyk, L. (1987) InInteractions of Water in Ionic and Nonionic Hydrates, H. Kleeberg (ed.) (Springer Verlag, Berlin Heidelberg), pp. 283–286.

    Google Scholar 

  • Sobczyk, L. (1988)J. Mol. Struct. 177, 111–124.

    Google Scholar 

  • Walker, N., and Stuart, D. (1983)Acta Crystallogr. A39, 158.

    Google Scholar 

Download references

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Authors and Affiliations

  1. Institute of Chemistry, University of Wrocław, F. Joliot-Curie 14, 50-383, Wrocław, Poland

    Z. Malarski & T. Lis

  2. Institute of Fundamental Chemistry, Technical University, 71-065, Szczecin, Poland

    E. Grech

Authors
  1. Z. Malarski
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  2. T. Lis
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  3. E. Grech
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Malarski, Z., Lis, T. & Grech, E. Crystal structure and IR spectra of the molecular complex of 5,6,7,8-tetrahydroquinoline with pentachlorophenol. Journal of Crystallographic and Spectroscopic Research 21, 255–259 (1991). https://doi.org/10.1007/BF01156074

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  • DOI: https://doi.org/10.1007/BF01156074

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