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Synthesis of deuterated methyl 2,3,4,6-Tetra-o-methyl-β-d-galactopyranosides

  • Organic Chemistry
  • Published:
Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

We have synthesized methyl 2,3,4,6-tetra-O-methyl-β-D-galactopyranosides selectively labeled with deuterium in positions 1–6 with deuterium content >90%.

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Literature cited

  1. N. K. Kochetkov, O. S. Chizhov, and B. M. Zolotarev, Izv. Akad. Nauk SSSR, Ser. Khim.,1967, 537.

  2. A. A. Solov'ev, V. I. Kadentsev, and O. S. Chizhov, Izv. Akad. Nauk SSSR, Ser. Khim.,1976, 2256.

  3. O. Gabriel, Carbohydr. Res.,6, 319 (1968).

    Google Scholar 

  4. Ph. Gorin, Can. J. Chem.,52, 458 (1974).

    Google Scholar 

  5. N. K. Kochetkov and B. A. Dmitriev, Izv. Akad. Nauk SSSR, Ser. Khim.,1964, 2095.

  6. M. Barczai-Martos and F. Körösy, Nature,165, 369 (1950); W. Koenigs and E. Knorr, Ber.,34, 957 (1901); G. Zemplen and E. Pacsu, Ber.,62, 1613 (1929).

    Google Scholar 

  7. A. Stoffin and P. Stoffin, J. Org. Chem.,32, No. 2, 4001 (1967).

    Google Scholar 

  8. D. J. Bell and S. Williamson, J. Chem. Soc.,1938, 1196.

  9. N. S. Williams and R. W. Jeanloz, J. Org. Chem.,29, 3434 (1964).

    Google Scholar 

  10. E. B. Rathbone, A. M. Stephen, and K. G. R. Pachler, Carbohydr. Res.,21, No. 1, 83 (1972).

    Google Scholar 

  11. M. Miljković, M. Gligorijević, and D. Miljković, J. Org. Chem.39, 2118 (1974).

    Google Scholar 

  12. H. J. Koch and A. S. Perlin, Carbohydr. Res.,15, 403 (1970).

    Google Scholar 

  13. R. Kuhn, T. Trischman, and J. Low, Angew. Chem.,67, 32 (1955).

    Google Scholar 

  14. A. C. Neish, Can. J. Chem.,32, 334 (1954).

    Google Scholar 

  15. T. Purdie and J. C. Irvine, J. Chem.Soc.,83, 1021 (1903).

    Google Scholar 

  16. A. Ya. Ott and O. S. Chizhov, Izv. Akad. Nauk SSSR, Ser. Khim.,1977, 201.

  17. L. Luckett and F. Smith, J. Chetn. Soc.,1940, 1506.

  18. D. J. Bell, J. Chem. Soc.,1940, 1543.

  19. G. O. Aspinall and P. E. Barron, Can. J. Chem.,50, 2203 (1972).

    Google Scholar 

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Authors and Affiliations

  1. N. D. Zelinskii Institute of Organic Chemistry, Academy of Sciences of the USSR, Moscow

    A. Ya. Ott & O. S. Chizhov

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  1. A. Ya. Ott
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  2. O. S. Chizhov
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 1, pp. 192–195, January, 1978.

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Ott, A.Y., Chizhov, O.S. Synthesis of deuterated methyl 2,3,4,6-Tetra-o-methyl-β-d-galactopyranosides. Russ Chem Bull 27, 168–171 (1978). https://doi.org/10.1007/BF01153233

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  • DOI: https://doi.org/10.1007/BF01153233

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