Summary
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1.
A number of new alkylphosphonothioic dichlorides were prepared from products of the oxidative phosphorylation of hydrocarbons.
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2.
Alkylthionophosphine Sulfides were synthesized in accordance with the scheme: hydrocarbon RH → alkylphosphonic dichloride RP(O)C12→alkylphosphonothioic dichloride RP(S)Cl2→alkylthionophosphine sulfide RPS2.
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In conclusion, we express our thanks to V. K. Gonik for molecular weight determinations.
Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 9, pp. 1619–1623, September, 1965
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Grishina, O.N., Bezzubova, L.M. Alkylthionophosphine sulfides. Communication 1. Synthesis and properties of alkylthionophosphine sulfides. Russ Chem Bull 14, 1581–1583 (1965). https://doi.org/10.1007/BF01083802
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DOI: https://doi.org/10.1007/BF01083802