Skip to main content
Log in

A vapor collection and thermal desorption method to measure semiochemical release rates from controlled release formulations

  • Published:
Journal of Chemical Ecology Aims and scope Submit manuscript

Abstract

Chemicals (bp 270–490 °C/1 atm) evaporated from a controlled-release formulation dispenser were carried by an airflow to a collector packed with a polymeric adsorbent. After a set time, the chemicals were recovered by thermally desorbing them onto a gas-liquid chromatograpic column. They were then separated and quantified. The apparatus is described, and the requirements for its successful use are discussed. The soundness of the thermal desorption technique was confirmed by comparison with another technique: solvent elution from the collector. The advantages of the former technique are discussed.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  • Cross, J.H., Tumlinson, J.H., Heath, R.R., andBurnett, D.E. 1980. Apparatus and procedure for measuring release rates from formulations of lepidopteran semiochemicals.J. Chem. Ecol. 6:759–770.

    Google Scholar 

  • Dietrich, M.W., Chapman, L.M., andMieure, J.P. 1978. Sampling for organic chemicals in workplace atmospheres with porous polymer beads.Am. Ind. Hyg. Assoc. J. 39:385–392.

    Google Scholar 

  • Fenimore, D.C., Davis, C.M., Whitford, J.H., andHarrington, C.A. 1976. Vapor phase silylation of laboratory glassware.Anal. Chem. 48:2289–2290.

    Google Scholar 

  • Ligon, W.V., andJohnson, R.L. Jr. 1976. Device for thermally induced vapor phase transfer of adsorbed organics directly from an adsorbent to a gas chromatograph-mass spectrometer.Anal. Chem. 48:481–484.

    Google Scholar 

  • Mieure, J.P. 1976. Porous polymer sorbents for analysis of organic air pollutents, pp. 121–128,in NIOSH Solid Sorbents. HEW Publ. PAO 059001. Washington, D.C.

  • Peterson, H., Eiceman, G.A., Field, L.R., andSievers, R.E. 1978. Gas chromatographic injector attachment of a porous polymer sorption trap.Anal. Chem. 50:2152–2154.

    Google Scholar 

  • Sydor, R., andPietrzyk, D.J. 1978. Comparison of porous copolymers and related adsorbents for the stripping of low molecular weight compounds from a flowing air stream.Anal. Chem. 50:1842–1847.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Additional information

Mention of a commercial or proprietary product in this paper does not constitute an endorsement of that product by the USDA.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Cross, J.H. A vapor collection and thermal desorption method to measure semiochemical release rates from controlled release formulations. J Chem Ecol 6, 781–787 (1980). https://doi.org/10.1007/BF00990402

Download citation

  • Received:

  • Revised:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00990402

Key words

Navigation